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Our technical resources XPS / ESCA analysis in a laboratory What do we mean by XPS analysis ? X-Ray Photoelectron Spectroscopy (XPS) is an analytical tool used to determine the chemical composition of a material to a depth of a few nanometers (XPS was previously known as ESCA, standing for Electron Spectroscopy for Chemical Analysis).The technique consists of irradiating the surface of a sample with an X-ray beam to then study the photoelectrons generated by the interaction between the beam and the material. Studying of photoelectrons makes it possible to determine the chemical composition of the material’s surface and to determine each element’s chemical environment (chemical bonds, oxidation number…). XPS is therefore a technique used to analyze the outermost surface (depth of 3 to 10 nm) of a material, making it possible to qualitatively and quantitatively determine its composition and the chemical forms of elements present on the sample’s surface Your needs : to determine the chemical composition of a sample’s surface Whatever your field, XPS analysis can fulfil your needs for surface analysis : XPS analysis as part of the development of a new product needing important surface functionalization (surface needing to adhere to a greater assembly, surface treatment to improve resistance to corrosion, wear, abrasion, etc.). Identification of the nature of a deposit or pollutant found on the surface of a material (elemental diagnostics and chemical forms) XPS analysis of the compliance of a surface treatment applied to an alloy to provide protection from oxidation (passivation, anodization…) These surface analysis will allow you to ensure the compliance of your products and to solve your industrial problems linked to defects (corrosion, discoloration…) and identify pollutants. Our solution : to provide XPS analysis suited to your requests and to deliver quick and reliable results FILAB is a multidisciplinary laboratory providing analytical services, some of which are ISO 17025 accredited : Characterization of the elemental composition of a material’s outermost surface Elemental identification by XPS Expert failure analysis (corrosion, apparition of a stain, discoloration…) Optimization of the passivation procedure as part of a development project XPS analysis Diagnostic of the nature of a deposit or contaminant Validation of a surface treatment process (anodization, passivation…) improving specific surface properties (resistance to corrosion, wear, etc.) Demander un devis What equipment is used in XPS analysis? XPS (X-ray Photoelectron Spectroscopy) analysis uses a variety of equipment to perform measurements and analysis. Equipment commonly used for XPS analysis includes the following: X-ray source: A piece of equipment generates X-rays, usually using an aluminum or magnesium anode. The X-rays emitted interact with the sample, causing electrons to be ejected from its surface. Photoelectron spectrum analyzer: An analyzer is used to measure the energies of electrons ejected from the sample as a result of interaction with X-rays. The most commonly used analyzers are hemisphere energy analyzers (HSA) and cylinder energy analyzers (CSA). Sample: The sample is placed in the vacuum chamber and exposed to X-rays. It may be solid materials or surfaces. The sample can be prepared by cleaning, polishing or fracturing, depending on the nature of the analysis required. Vacuum chamber: XPS analysis is performed in a vacuum chamber to avoid contamination of the sample by airborne molecules or particles. A high vacuum pressure is maintained inside the chamber during analysis. Detector: A detector is used to measure the number of electrons ejected at different energies. The most commonly used detectors are electron multiplier detectors (SEM) and microchannel anode detectors (MCP). Data acquisition and control system: A data acquisition and control system is used to control equipment, collect data and perform analysis. Specific software is used to process the data and interpret the spectra obtained. This equipment is used in combination to carry out XPS measurements, which enable analysis of the chemical components present on the sample surface, their oxidation state and their depth distribution. Differentiating between XPS analysis and XPS characterization XPS characterization and XPS analysis are common techniques in materials science and chemistry. Although both involve the use of photoelectron spectroscopy, there are some key differences. XPS characterization is used to determine the chemical elements present in a sample, their percentages and molecular structures. XPS analysis, on the other hand, is a more in-depth study of these elements, including their electron charge distribution. Ultimately, XPS characterization is useful for identifying elements in a sample, while XPS analysis provides more detailed information on their electrical behavior. By understanding these differences, researchers can make effective use of these techniques in their research.  Learn more about XPS characterization XPS characterization, or X-ray photoelectron spectroscopy, is a surface analysis technique widely used in materials science. It can be used to study the chemical composition, electronic structure and interactions between atoms on the surface of different types of materials, such as metals, oxides, polymers and semiconductors. This method relies on the interaction between high-energy photons and surface electrons, which are then measured to provide valuable information on material properties. XPS characterization is a non-destructive, highly sensitive technique that can be used for a variety of applications, from fundamental research to materials characterization in industry. FAQ How does XPS analysis work? XPS analysis works by irradiating the sample with X-rays, causing electrons to be ejected from its surface. The ejected electrons are then analyzed in terms of kinetic energy to determine the chemical elements present and their oxidation states. What types of samples can be analyzed by XPS? XPS analysis is applicable to a wide range of materials, including metals, semiconductors, polymers, ceramics and composites. Samples must be solid and stable under vacuum. What are the benefits of XPS analysis? XPS analysis offers advantages such as high chemical sensitivity, the ability to analyze surfaces non-destructively, the possibility of quantitative analysis and the detection of chemical species present on the surface. What are the limitations of XPS analysis? Limitations of XPS analysis include the need to prepare solid samples, the inability to analyze thick layers of materials, the influence of surface properties on results, and the complexity of data interpretation. How is a typical XPS analysis performed? A typical XPS analysis involves sample preparation, introduction of the sample into a vacuum chamber, irradiation with X-rays, collection of the ejected electrons, their analysis in terms of kinetic energy and interpretation of the data obtained. What are the applications of XPS analysis? XPS analysis is widely used in many fields, such as materials science, electronics, catalysis, corrosion, nanotechnology, surface biology and coatings research. To fulfil your needs for XPS analysis, FILAB offers multisectoral expertise and a cutting-edge analytical fleet to reliably fulfil the various requests coming from industrial clients.For more information about our laboratory’s elemental analytical services, feel free to contact us ! Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Chemical expertise in a laboratory Your needs: to carry out an expertise using scientific data and technical interpretations. In order to face complex challenges, you are looking for an independent and impartial laboratory to carry out an expertise using specific techniques which will allow you to asses a given uncertainty.Expertise is a decision-making process that calls upon technical or scientific examinations in order to evaluate or assess a given subject. It leads to an interpretation, a recommendation or an opinion based on concrete evidence. Our solution: to assist experts with reliable analysis and scientific interpretations. FILAB provides services to industry by providing its expertise in Chemistry and Materials Science, its cutting-edge analytical fleet and the know-how of its highly trained staff made up of doctors and engineers to assist in solving expertise problems.Our multidisciplinary technical skills allow us to accommodate for a wide range of requests, which we handle with impartiality and total confidentiality.FILAB provides its expertise skills for the following services: Our Services Metal part expertise Material expertise Surface expertise Metallurgical expertise Failure expertise : coating peeling off, adhesive problems, deposits, fissures...  Chemical analysis Our means Organic analysis : GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Powder analysis : XRD, SEM-EDX, BET Metallurgical analysis : ICP, SEM-EDX, SEO Thermal analysis : TGA, DSC Mineral analysis : ICP, DRX, CI Surface analysis : SEM-EDX, XPS, TOF-SIMS
Sectors of activity Laboratory analysis of luxury goods Your needs : to design luxury products using high quality materials. Major brands, manufacturers and subcontractors in the luxury industry are all subject to common priorities and requirements : the pursuit of zero defects, higher production speed, better assembly reliability and the use of high-quality, durable materials.In order to meet these challenges specific to the luxury industry, inspection of the materials used is an essential step. Several factors can affect the life cycle of a luxury product :Defective raw materialsNon-conforming raw materialsAppearance of defects in the final productProblems in the suppliers' production process leading to delays in deliveryetc.For assistance with these industrial challenges you are searching for a reliable, independent laboratory with high added technical value. Our solution : to offer tailored assistance to luxury industrialists by combining analytics, expertise and counselling on the design of their products. FILAB laboratory being specialized in analysis and material characterization, has been assisting luxury industrialists in designing and inspecting their products using analytical techniques specific to their needs.Based on experience and its state-of-the-art analytical equipment, FILAB has a wide range of accurate and reliable tools at its disposal to provide the following services : ANALYSIS Chemical analysis (raw materials, finished products)) Packaging analysis Precious metal analysis REACH analysis Material characterization : polymers, leather, metals, composite materials, ceramics… Powder analysis Surface analysis and coating thickness measurements Nickel release test EXPERTISE Expert chemical analysis Compatibility studies (container/contents interactions, extractables and leachables) Pollutant identification using SEB or FTIR Failure analysis : ruptures, corrosion, coloring and odor problems, etc. Laboratory audit et analytical training Deformulation services R&D Creation and transfer of analytical techniques Research into substitutions for allergenic or toxic raw materials Industrial project development R&D assistance (Literature review, project management, choice of materials…) Creation of an innovative product OUR FACILITIES Organic analysis : GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Mineral analysis : ICP, XRD, IC Thermal analysis : TGA, DSC Metallurgic analysis : ICP, SEM-FEG EDX, OES Powder analysis  : XRD, SEM-FEG EDX, BET Surface analysis : SEM-FEG EDX, PES, TOF-SIMS
Sectors of activity Laboratory tests and analysis for the automobile industry Your needs : to design and manufacture reliable and efficient automobile equipment As steel producers, smelters, plastic producers, manufacturers, tier 1 suppliers or subcontractors for the automobile industry you are confronted on a daily basis with the stringent specifications for the quality and reliability of the materials used in automobile assemblies.In an industry undergoing significant change and facing major strategic challenges (ecology, passenger safety, competition, etc.) you are looking to :Inspect your raw materialsDevelop new, more robust, and more efficient materialsOptimize your manufacturing and machining processesImprove the effectiveness of surface treatmentsExamine the performance and the lifespan of your materials Our solution : to assist automobile industrialists in analyzing and improving their materials FILAB is an independent laboratory located in Dijon, France, with an analytical fleet spread over 5 200m² and has extensive experience in assisting projects for the automobile industry.FILAB offers its analytical expertise and R&D counselling for the following services :  ANALYSIS Custom chemical analysis : fluids, additives, impurities, heavy metals… Metallic alloy inspection Surface treatment analysis and surface treatment baths REACH analysis Material characterization : polymers, metallic alloys, composite materials, glass, ceramics… Surface analysis and coating thickness measurements Determination of residual solvents and VOC using GC-MS EXPERTISE Expert chemical analysis Deformulation services Failure analysis : fissures, particular contamination, adhesive problems, corrosion, metallographic inspection, weld analysis… Assistance in optimizing the manufacturing process Compatibility studies between certain materials and fluids Laboratory audit and analytical training R&D Creation, validation and transfer of analytical procedures R&D assistance (Literature reviews, project management, choice of raw materials…) Research into substitutions for substances Developing a new formula or a new substance OUR FACILITIES Organic analysis : GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Thermal analysis : TGA, DSC Powder analysis : XRD, SEM-FEG EDX, BET Mineral analysis : ICP, XRD, IC Metallurgic analysis : ICP, SEM-FEG EDX, SEO Surface analysis : SEM-FEG EDX, PES, ToF-SIMS Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Sectors of activity Analytical services for the cosmetics industry Your needs: to evaluate the quality of your cosmetic products in the context of a new product launch or a change in regulations The cosmetics industry is often associated with high expectations in terms of efficiency, stability and safety for a finished product. As major players in the production of cosmetic products, as subcontractors or as producers of raw materials, you regularly need to adapt your production processes to follow the changes in regulations.Analysis can be necessary to verify the conformity of a cosmetic product or to identify the cause of a product failure.To overcome these challenges, you are looking to cooperate with a reliable and independent analytical laboratory offering high added technical value.  Our solution: to develop your analytical techniques, to analyze the chemical composition of cosmetic products or to characterize failures using the relevant techniques The FILAB laboratory, made up of experts in cosmetic analysis and defect characterization, can offer its analytical services throughout the designing and production processes all the way to the process of putting the product on the market (makeup, crème, perfume…).FILAB is ISO 17025 accredited by COFRAC for the analysis of heavy metals in cosmetic productsContact FILAB for cosmetic analysisRelying on experience and our cutting-edge analytical fleet, the FILAB laboratory has a wide range of tools specific to the cosmetics industry which allow us to provide the following services: ANALYSIS Analysis of undesirable substances found on raw materials or finished products: heavy metals, residual solvents, phthalates, bisphenol A… Determination of preservatives (phenoxyethanol, parabens, chlorphenesin using HPLC-UV, HPLC-MSMS and GC-MS Siloxane (D4/D5) analysis Powder analysis: PSD, specific surface area measurements, morphology, crystallinity… REACH analysis Determination of UV filters    Determination of active ingredients: organic and mineral solar filters, vitamins Packaging analysis: polymers, composite materials, glass Thermal analysis Metallurgic analysis Analytical validation following ISO 12787 EXPERTISE Non-conformity expertise: particulates, deposits, unknown spikes, material degradations… Optimization of your production procedures Failure analysis: fractography, particulate contamination, adhesive problems, corrosion, metallographic examination, weld analysis… Deformulation services Compatibility analysis (container/contents interactions, extractables and leachables) Laboratory audit and analytical training R&D Creation, validation and transfer of analytical procedures Literature reviews Research into substitutions for substances Developing analysis kits OUR FACILITIES Organic analysis : GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Thermal analysis : TGA, DSC Powder analysis : XRD, SEM-FEG EDX, BET Mineral analysis : ICP, XRD, IC Metallurgical analysis : ICP, SEM-FEG EDX, SEO Surface analysis : SEM-FEG EDX, PES, ToF-SIMS Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure What is composition analysis of a cosmetic product ? The analysis of the composition of a cosmetic product in a laboratory is a technique used by professionals in the cosmetic industry to evaluate the chemical composition of a product. This analysis makes it possible to determine the proportions of the different ingredients present in the product: preservatives, emulsifiers, colorants, perfumes, essential oils ...This also makes it possible to ensure that the product complies with the regulations in force in the cosmetic industry, and to guarantee its safety for consumers. The results can also help to improve the formulation of the product and improve its performance. Is FILAB registered with the FDA (Food and Drug Administration)? Yes, as an industrialist if you wish to export your cosmetic products FILAB is able to meet your analysis needs.Find the registration certificate d'enregistrement
Our services Laboratory analysis and expertise of surface treatments Your needs : to characterize a defect found in your surface treatments and coatings With the aim of better protecting a material’s surface from its environment, surface treatments bring new physicochemical properties to the material, giving it better resistance to corrosion, wear and tear, etc. Surface treatments can also be used for visual purposes, changing the overall appearance of a material.There are various techniques used to treat surfaces : techniques Wet surface treatments : chemical baths (chemical nickel, copper…), electrolytical deposits, galvanization… Dry surface treatments : thermal spraying, plasma, chemical or physical vapor deposits (CVD and PVD), sandblasting… These organic or metallic treatments can be subject to a number of challenges regarding defects  (adhesive problems, peeling, degradation…) occurring over time due to an incompatible environment. FILAB provides industrialists with the means to detect and understand these defects. Our solution : to optimize your surface treatments and coatings to ensure their proper functionality Thanks to our dual expertise in chemistry and materials science, FILAB laboratory provides analytical services on all kinds of surface treatments (organic and inorganic), and all types of materials (metals, glass, polymers, ceramics…).Our laboratory can resolve your problems relating to industrial surface treatments by providing the following services : Our services Analysis of surface treatment baths Coating thickness measurements Hot-dip galvanization services Defect expertise Surface coating characterization Detection and characterization of impurities (deposit, pollutant, particulate…) Surface analysis Our facilities for analyzing and characterizing surface treatments are also quite diverse depending on the type of treatment : Scanning Electron Microscope (MEB-FEG-EDX), ToF-SIMS analysis, XPS for morphological examinations : ICP-AES, ICP-MS or Ionic Chromatography for analyzing chemical compositionsIf you need more information about our analysis of surface treatments, feel free to contact us !
Sectors of activity Analytical laboratory working with the energy and nuclear industries Your needs : to develop efficient procedures and reliable products to meet environmental challenges. Being subject to the tough challenges facing sustainable energy and the need to protect the environment, you are looking to optimize your products, materials or procedures according to quality, sustainability and security practices. As major players in the designing, construction, maintenance and operation of nuclear stations or other energy production systems you are trying to abide by these practices by routinely inspecting your raw materials and other products or materials used in the process with the aim of correcting any failures.To support you in your efforts, assistance from a laboratory specialized in analysis and characterization, certified by recognized authorities, will allow you to reliably evaluate the conformity of your products. Our solution : to assist industrialists in the energy sector in improving their materials with quality control and analysis. FILAB’s expertise in the fields of energy production and of nuclear energy contribute towards the advancement of your industrial projects in terms of inspection, optimization and counseling services regarding your activities.For many years now FILAB has been approved by EDF to perform the necessary analysis for “PMUC” product registration and “PMUC” inspections.From the start of the designing process to the commissioning of your facilities, FILAB assists you in assessing compliance with international requirements by providing the following services : ANALYSIS Chemical analysis (heavy metals, additives, residuals solvents …) Material characterization : polymers, metals, composite materials, ceramics… Determination of heavy metals and residual solvents REACH analysis Analysis of products used in nuclear stations (EDF approval) Surface analysis Powder analysis EXPERTISE Compatibility studies between certain fluids and materials Deformulation services Failure analysis : fissures, particulate contaminants, adhesive failures, corrosion, metallographic examination, weld analysis Identification of unknown pollutants (deposits, particles) Stability analysis Laboratory audit and team training R&D Development and validation of new analytical techniques Research into substitutions for CMR substances Developing a new substance Literature reviews R&D assistance (project management, choice of materials…) OUR FACILITIES Organic analysis : GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Thermal analysis : TGA, DSC Powder analysis : XRD, SEM-FEG EDX, BET Mineral analysis : ICP, XRD, IC Metallurgical analysis : ICP, SEM-FEG EDX, OES Surface analysis : SEM-FEG EDX, PES, ToF-SIMS Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Laboratory analysis of nanomaterials for the cosmetics industry Reminder: what does the EC Regulation 1223-2009 on Cosmetics state ? Mainly used as UV filters, pigments, mattifiers, rheological agents or opacifiers, nanomaterials are regularly used in cosmetic products whether that be intentionally with the aim of using their specific properties or whether it be unintentionally.The 2009 Cosmetic Regulation pays particular attention to the use of nanoparticles, nanomaterials or any other form of nanotechnology in cosmetic products.A nanomaterial is defined by the EC regulation 1223-2009 on cosmetics as an insoluble or bio-persistent material, made intentionally and characterized by one or more external dimensions, or by an internal structure, on the scale of 1 to 100 nanometers.The Cosmetics Regulation therefore states that : - Nanomaterials must be specifically labeled (must have [nano] in the ingredients list preceded by the INCI ingredient name)- Cosmetic products containing nanomaterials must be registered with the European Commission via the CPNP (articles 13 & 16) 6 months before going to marketAt the national level in France, the R-Nano declaration requires that the of nanomaterials be traceable. Whether their use is intentional or not, the use of nanomaterials  must be declared and traceable through physicochemical characterization services. Regarding the unintentional use of nanoparticles, the main suspicions surround raw materials such as metal oxides and mineral materials (TiO2, ZnO, SiO2, Fe2O3, CaCO3...). FILAB can assist you in analyzing nanoparticles found in your cosmetic products FILAB provides a compilation of services centered around nanomaterials, namely those found in the cosmetics industry. Our laboratory is equipped with many machines capable of characterizing nanomaterials.Detection of nanoparticles and nanomaterials in cosmetic productsNanometric classification of raw materials and finished productsChemical composition analysis of nanoparticle-based products and trace residue analysis (ICP-AES, ICP-MS)Nanoparticle size and shape determination by SEMCount and particle size distribution measurement by SEM, DLS, Laser GranulometryCharacterization of nanoparticles’ surfaces, Zeta Potential, TGA, SEM, FTIR, Raman, ToF-SIMS, XPSBET specific surface area measurement and Helium Pycnometry density measurementDevelopment and validation of analytical methods specific to nanomaterialsContainer/Contents interaction testingNanoparticle detection by SP-ICP-MS or A4F-ICP-MSLiterature and regulatory reviewsAnalytical training 
Our services Laboratory analysis of outermost surface layers From surface analysis to outermost layer analysis  Material’s surface is subject to numerous interactions with its environment and dictates the specific characteristics, performance of materials as well as providing protection from exterior constraints.Surface analysis can help resolve many physicochemical problems:https://www.youtube.com/watch?v=Azphz1DMmAkAs part of an expertise to determine the origin of a defect (corrosion, fissure, adhesive problem, unknown pollution…)To optimize your production processes (surface treatment, machine calibration…) and improve the performance of your materialsTo inspect the quality of the surface of your materials  Outermost surface analysis : more specific chemical characterization Complementary to surface analysis techniques (SEM, Optical microscopy…), techniques associated with outermost layer analysis used to collect specific data identifying chemical elements and molecules in a materials surface and its close environment.They are used as part of multisectoral investigations such as :Identification of the chemical nature of a pollutant or a contaminant which could cause cleanliness problemsSurface characterization (passivation and functionalization)  Our analytical services FILAB laboratory has multisectoral expertise as well as a cutting-edge analytical fleet allowing us to reliably fulfil our clients’ requests for outermost layer analysis.Our laboratory is able to use many complementary analytical techniques :AFMTOF-SIMSXPS/ESCAOur skills in chemistry and materials science ensure a reliable level of expertise for all your analytical needs. Examples of problems we have solved in various fields Medicine :Inspection of the cleanliness of a Medical Device’s surface as part of the validation process for a cleaning procedureDetection of residual detergents on the surface of an implant using complementary ToF-SIMS and XPS techniquesCharacterization of the surface of a Medical Device : morphology, elemental composition, molecular characterization, detection of contaminants…Aeronautics/Automobiles :Examination of an adhesion problems in paint (XPS or FESEM elemental identification, ToF-SIMS molecular analysis…)Identification of a sizing product found on the surface of fibers used to make composite materialsCharacterization of an aluminum alloy passivation procedure Electronics :Identification of a pollutant found on the contact surface of a glued assembly creating an adhesive problemFailure analysis following a loss in performance Pharmaceuticals :Identification of a contaminant found on the internal surface of a glass bottleOutermost layer characterization of packaging with a sealing problem          
Our services Laboratory of silicone testing and analysis What do we mean by silicones ? Silicones are polymers structured around a siloxane bond and make up a wide variety of materials. Their consistency does vary, they can be liquids, hard plastics, gels or even rubber. They can be found almost everywhere in our daily lives as mastics, glues, joints, anti-foaming agents in detergent powders, cosmetics, medical equipment, insulating sleeves, electrical cables. How can FILAB assist you in characterizing your silicone-based samples ? FILAB laboratory uses many material characterization techniques which rely on different physicochemical principles. FILAB provides the following services :Chemical composition analysis of siliconeStudy of the thermal properties of silicone using DSC and TGADetection of impurities in oils or silicone fluidsDetermination of the silicone and siloxane contents in industrial matricesFailure analysis of silicone : odor problems, discoloration, pollution, degradation…   Our equipment for silicone testing Organic chemical analysis : GC-MS, Py-GC-MS, LC-MS/MS, GPC, NMR, FTIRInorganic chemical analysis : ICP, XRD, ICThermal analysis : TGA, DSC, Py-GC-MS, ATG-FTIRPowder analysis : XRD, SEM-FEG-EDX, BET, Laser GranulometrySurface analysis : SEM-FEG-EDX, XPS, ToF-SIMS 
Our services Surface coatings characterization and analysis laboratory Your needs : to characterize a surface coating following the detection of a defect or after a change in regulations What is a surface coating ? A coating is a layer of organic or metallic material designed to improve the surface properties of a product to made said product more resistance to outside constraints. In doing so, coatings can be used to preserve the appearance of a product, to protect it from corrosion, from ware or changes in temperature or even to improve its adhesive properties.Surface coatings can be applied to various types of materials : polymers, metals, ceramics… Why analyze a surface coating ? The reliability of a material is directly linked to its surface properties. The cause of defects such as ruptures, wear or the apparition of a stain can be traced back to the quality of the coating that was applied to the product. Analysis and characterization of the coating as well as a measurement of its thickness will allow us to determine its chemical composition and to verify that it complies with standards.Assistance from an analytical laboratory using techniques specific to the study of coatings will allow you to improve the quality and efficiency of your product while complying with increasingly stringent environmental and regulatory restraints. Our solution : to determine the cause of surface coating degradations using specific techniques Our services Relying on its expertise in dealing with surface treatments for organic and metallic elements, FILAB laboratory can assist you in carrying out failure analysis of the coating by providing various services :Layer identification and characterization (coatings, surface treatments, deposits…)Coating thickness measurementsDetection and analysis of impuritiesAccelerated aging testsR&D assistance : choice of materials or of production procedureFor these types of services, FILAB laboratory uses cutting-edge analytical techniques such as Scanning Electron Microscopy coupled to an EDX microprobe (SEM FEG EDX) or ToF-SIMS, XPS, AFM analysis, and more… Why FILAB ? As an independent laboratory with a team made up of highly qualified personnel, FILAB guarantees the reliability of its results, a quick turnaround for requests and tailored support for clients.
Our services Analysis and determination of cleaning residue : THC, TOC and detergent residue on Medical devices FILAB is the first laboratory to be ISO 17025 accredited by COFRAC for TCH and TOC analysis of Medical Devices and Equipment in accordance with the ISO 19227 set (previously known as NF S94-09) Your needs : to have your MD cleaning procedures validated in accordance with relevant standards The cleaning process is crucial when manufacturing medical implants. With the aim of eliminating any residual contaminants, the manufacturer of a medical device must adapt the cleaning process to their own needs or to those of their client by precisely identifying the type of contaminant involved in the manufacturing process of the implant, in the way it’s going to be handled and in the way it will packaged and stored (lubricants, particulates, detergent residue, inorganic residue…)Among other things, the NF S94-091 standard defined which factors needed to be taken into account when validating the cleaning process which orthopedic implants undergo before being packaged.The development and implementation of specific analytical techniques (determination of heavy metals, THC and TOC analysis) is a key step in evaluating the cleanliness of medical implants. Our solution : to provide you with our know-how and our COFRAC certified analytical tools to help develop and validate your cleaning procedures FILAB is ISO 17025 accredited by COFRAC for Total HydroCarbons (THC) analysis and Total Organic Carbons (TOC) analysis of Medical Devices and Equipment in accordance with the ISO 19227 set (previously known as NF S94-09) :-        ISO 9377-2 for THCs-        EN 1484 for TOCsWe are therefore the first laboratory in France to be ISO 17025 accredited for medical devices. For more information visit : www.cofrac.frOur experts are at your disposal and offer their analytical services for cleaning residue, THC, TOC, detergent residue, acids and heavy metals :THC analysis of  Medical Devices (orthopedic implants, implantable devices…) using GC in accordance with ISO 9377-2 (THCs : presence of lubricants, cutting oil…)TOC analysis of Medical Devices (orthopedic implants, implantable devices…) using a TOC-meter in accordance with EN 1484HCT / COT dissolution, extraction in accordance with ISO 10993-12 or lixiviation analysisValidation of cleaning procedures in accordance with ISO 19227:2018Analysis according to astm f2459Evaluation of the efficiency of an extraction technique in accordance with ISO 10993-12Analysis and determination of detergent residue using ICP and Ionic ChromatographyAnalysis and determination of inorganic residue using ICP and Ionic ChromatographyAcid analysis using ICP and Ionic ChromatographyResidual analysis of aluminum based polishing pasteBiocompatibility testing in accordance with ISO 10993-18Analytical development for determining THCs and TOCs on Medical devicesAnalytical validation for determining TCHs and TOCs on DMsAnalytical services and validation in a laboratorySurface and extremity analysis using XPS and/or ToF-SIMSUnknown pollutant analysis (embedded or not)Identification and quantification of potential degradation products in accordance with the ISO 10993 set
Our technical resources ToF-SIMS analysis in a laboratory Your needs: characterize the extreme surface chemical composition of a sample using TOF-SIMS analysis What is TOF-SIMS ? Time-of-Flight Secondary Ion Mass Spectrometry (ToF-SIMS) is an imaging and analysis technique for obtaining elemental and molecular information on the species present at the extreme surface of solid-state samples.In short, it provides information on the sample's chemical composition, spatial distribution of elements and chemical bonds.This technique can be applied to a wide variety of materials, including polymers, metallic materials, ceramics, and composite materials, films, glass and fiberglass, ceramics, dental implants, ... without requiring complex sample preparation. Why perform TOF SIMS analysis in the laboratory ? TOF SIMS analysis is particularly valued for its ability to provide detailed information on the chemical composition of materials at both surface and depth (down to 1nm).Not only can the surface be examined to identify the elements and molecules present, but depth profiles can also be produced by progressively removing layers, thus revealing compositional variations at different levels. What sets this technique apart is its ability to identify the molecular structure of compounds.This dual analysis capability, spatial and molecular, makes TOF SIMS analysis indispensable for surface studies, the study of interactions between materials, the understanding of the presence of corrosion, the analysis of coatings and many other applications. TOF SIMS, state-of-the-art technology TOF SIMS analysis is a state-of-the-art technique offering high sensitivity and molecular resolution for extreme surface analysis and the study of the chemical composition of materials.TOF-SIMS analysis provides qualitative and semi-quantitative information on the elements and molecules present. In addition, it is a high-resolution imaging technique that can map the distribution of elements and molecules on the surface of a sample with high spatial resolution. This capability enables the FILAB laboratory to understand surface heterogeneities and material interfaces.ToF-SIMS is therefore a highly sensitive surface analysis technique, enabling detection limits of elements or molecules in the ppm range.All conductive and insulating materials stable under ultra-high vacuum can be analyzed by ToF-SIMS: metals, alloys, semiconductors, polymers, varnishes, paints, adhesives, additives, surfactants, ceramics, glass, wood, paper, textiles, ultra-high vacuum, thin deposits... Surface sensitivity of sims analysis The high sensitivity of the TOF-SIMS technique makes it an excellent initial tool for identifying the types of species present on a sample. Once sims analysis has been performed, other methods can be used to obtain more detailed information, such as XPS. What's more, sims analysis can detect species at much lower levels than traditional systems.In static SIMS analysis, a pulsed primary beam targets only the first monolayer of the sample. Unlike dynamic SIMS analysis, this approach preserves the molecular integrity of the surface. Molecules are simply desorbed or fragmented into several pieces. Secondary ions, made up of fragments of the original molecules, are then detected by a time-of-flight spectrometer. Molecular ions weighing up to 10,000 amu can be identified, providing detailed information on the molecular structure of organic compounds. Our solutions : offer TOF-SIMS analysis techniques specific to your requirements and deliver fast, reliable results Why choose FILAB ? The FILAB laboratory specializes in TOF-SIMS analysis for the study of the chemical and molecular composition of material surfaces. Adapted to sectors ranging from microelectronics to biotechnology, we combine expertise in extreme surface analysis and cutting-edge TOF SIMS technology to deliver accurate and reliable results, down to the nanoscale. Find out how our TOF-SIMS analyses can contribute to the success of your quality and innovation projects. Our solution : to provide ToF-SIMS analysis techniques specific to your requests with reliable results Our TOF SIMS analysis services L'analyse ToF SIMS ou l'expertise de la composition chimique élémentaire et moléculaire de l'extrême surface d'un échantillon peut être mise en œuvre dans différents contextes : ToF-SIMS expertise as part of an R&D project associated, for example, with the optimization of a bonded assembly (characterization of surface chemical functions) Identification of pollution or deposits on the surface of a material (elemental and molecular diagnostics) Verification of a product's surface function, enabling it to improve its performance in terms of adhesion, mechanical bonding, etc. Multilayer analysis Feasibility study Particle analysis Comparative study Atomic and molecular identification (0 to 10,000 amu) Detection of all elements down to ppm Qualitative analysis Isotope analysis Profiling an organic sample (argon aggregate) and maintaining molecular information at depth (3 µm - 10 µm max) Differentiating IS chemistry Paint delamination Determining the cross-linking rate of a “plasma polymer" Paint fading  These extreme surface analyses enable you to ensure the conformity of your products, and respond to industrial problems of failure and pollution identification. Industrial applications of TOF-SIMS technology TOF-SIMS analyses are in demand in various industries for their ability to characterize the chemical composition of surfaces with great sensitivity and resolution.In the semiconductor industry, this technique is used to monitor material purity and device structure, directly affecting the performance and reliability of electronic components.The pharmaceutical industry also takes advantage of TOF-SIMS for biocompatibility analysis, between medical device surfaces and the biological environment.In materials research, TOF SIMS is used to understand the surface properties of new composite materials, with targeted properties.In the energy sector, this technique is used to analyze materials for batteries and solar panels. Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure FAQ What are the principles of TOF SIMS analysis? Extreme surface analysis by TOF-SIMS involves first preparing the sample, then introducing it into the spectrometer's vacuum chamber. A beam of primary ions bombards the surface, releasing secondary ions which are then identified by their time-of-flight, enabling the chemical composition of the surface to be determined.The principle consists in bombarding the surface to be analyzed with a pulsed source of primary ions (Ga+, Bin+, Au+, C60+, ...) to produce secondary ions from the first monoatomic layers of the sample. These secondary ions, whether positive or negative, are then focused and accelerated in a time-of-flight analyzer, where their travel time is a function of their mass. Coupled with a scanning device for the primary ion beam, this provides a map of the various chemical elements and molecular species on the sample surface. What is the detection limit of TOF-SIMS? TOF-SIMS can detect elements at extremely low concentrations, down to levels of a few parts per million (ppm), depending on the sample matrix and experimental conditions.
Our services Laboratory analysis and expertise of surface coatings Your needs : to analyze and study the state of a coating on your products and materials as part of an R&D project or following a product failure What is a coating ? A surface coating is applied to a product or material to improve their surface properties (appearance, resistance, adherence, permeability…) and to protect them from environmental attacks. Coatings can be organic (polymer) or inorganic (metallic or ceramic) in nature. To modify the surface properties of a material to make it more compatible with its environment and the conditions in which it will be implemented, different methods can be used : Mechanical operations which work on existing material : burnishing, gumming, polishing… Chemical operations aiming to apply a solution to a product’s surface : varnish, paint, adhesive… Electrochemical operations or passivation / anodization systems, which seek to chemically modify a surface using a surface treatment bath  Why analyze a product’s coating ? Surface treatment operations are an essential step of R&D processes to determine the performance of a finished product and to ensure its longevity. The point of origin of product failures such as ruptures, wear or the apparition of a stain can be linked to the quality of a coating. Analysis and characterization of coatings make it possible to determine the chemical composition of layers and to verify their compliance and their performance. Support and assistance from an expert laboratory using techniques specific to the study of coatings will allow you to improve the efficiency and quality if your products while complying with environmental and regulatory constraints. Our solution : to carry out characterizations and expertise of your coating using specific techniques Thanks to expertise in surface treatments for organic or metallic elements, FILAB laboratory can assist you in analyzing defects found in the coating of a product by providing various services : Our services Chemical composition analysis of a coating Identification and characterization of surface layers (coatings, surface treatments…) Coating impurity analysis R&D support : choice of surface treatment or cleaning procedure Evaluation of the state of a surface and the homogeneity of surface elements Coating thickness measurements Accelerated aging tests To provide these services, FILAB laboratory uses cutting-edge analytical techniques such as Scanning Electron Microscopy coupled with an EDX microprobe (SEM FEG EDX) and outermost layer analysis techniques such as ToF-SIMS, XPS…
Sectors of activity Analytical laboratory serving the Pharmaceutical Industry The pharmaceutical sector is a world unto itself, with its own rules and codes. The FILAB laboratory fully understands this exceptional dimension. Our PhD students and engineers are trained to meet your specific needs for pharmaceutical analysis and expertise:Implementation of an analysis method specific to your products, validated to ICH Q2 standardsImpurity or particle identificationA behavioral problem with one of your products (degradation, color change, odor, etc.)Deformation of an existing API or productFrom the development of new galenic formulas to the control of your production, the FILAB laboratory offers you high-level human skills and state-of-the-art analytical equipment to provide you with tailor-made services, in a quality environment that meets GMP criteria. FILAB provides analysis and expertise for the pharmaceutical industry. As an extension of your in-house laboratories, the laboratory offerspharmaceutical manufacturers with the following services: Analysis Our control analyses for the pharmaceutical industry • Nitrosamine analysis Nitrosamine analysis Nitrosamines are classified by the IARC and WHO as harmful compounds that can cause cancer in humans. What's more, ANSM keeps a close eye on them. Discover our services • Elemental impurity detection according to ICH Q3D Elemental impurity detection according to ICH Q3D The ICH Q3D guide sets out the procedure for assessing elemental impurities in pharmaceutical products, including those intended for human use. Discover our services • Residual solvent analysis according to USP 467 (ICH Q3C context) Residual solvent analysis according to USP 467 (ICH Q3C context) The ICH Q3C guideline provides guidance on toxicologically acceptable thresholds for patient safety with regard to residual solvent concentrations (or residual volatile impurities) in pharmaceutical products. Discover our services • Solid analysis Solid analysis • Stability testing of pharmaceutical products and drugs Stability testing of pharmaceutical products and drugs Expertise Our expertise and R&D support • Particle contamination Particle contamination Particle counting is a crucial method for measuring and quantifying contaminants in various media, such as air, water and raw materials, and is vital in many scientific and industrial sectors. This technique provides detailed information on the size, shape and distribution of particles, which is particularly important for the pharmaceutical industry in monitoring the contamination of powders and injectable products. • Extractibles & Relargable / stability study Extractibles & Relargable / stability study Analysis of extractables and leachables enables us to check the conformity of health products, assessing the risks of substance migration from packaging. Discover our services • Degradation studies Degradation studies A forced degradation study tests the stability of pharmaceutical products/APIs to assess their behavior, purity and compliance over time. Discover our services • ICH Q2 analytical validation and development ICH Q2 analytical validation and development The ICH Q2 guideline for the validation of analytical methods, drawn up by ICH experts and subject to regulatory consultation. Discover our services In particular, FILAB is the only laboratory in France accredited to ISO 17025 by COFRAC (www.cofrac.fr: accreditation no. 1-1793) for the analysis of elemental impurities in pharmaceutical matrices. Our technical resources Organic chemical analysis GC/MS, Py-GCMS, UPLC-MSMS, LC-QTOF-MS, LC-QTOF-MS, LC-ORBITRAP, GPC, NMR, FTIR Powder analysis XRD, SEM-FEG EDX, BET, Laser granulometry Mineral chemical analysis ICP, XRD, IC Thermal analysis ATG, ATG-FTIR, DSC Surface analysis MEB-FEG EDX, XPS, TOF-SIMS
Our services Filab, materials characterization laboratory The FILAB laboratory offers a physico-chemical analysis and characterization service for all types of materials. Materials science studies the properties, structure, synthesis and manipulation of materials to create new materials with improved performance. The FILAB laboratory's engineers and PhDs are supported by technical resources located in the 5 200m² Analytical Park.Materials characterization is the process of evaluating and describing the physical, chemical, mechanical, thermal, electrical, optical, magnetic and other properties of materials. Why characterize materials? 01 Compatibility of the material with the product's end use 02 Evolution of the material over time or in the face of different environments 03 Conformity materials with respect to current standards 04 Performance of material Each material has its own characteristics, whose properties will govern the performance of the final product. Indeed, the criteria for choosing a material can affect its chemical nature, composition, shape (granulometry, crystallinity, morphology, etc.), surface finish and so on. From shaping to use of the final product, it is essential to ensure the conformity of the materials used and to control the risks of failure (cracks, breakage, corrosion, etc.).The support and experience of a laboratory specializing in material characterization or materials research enables you to optimize your production processes with more suitable materials, and to accurately analyze the causes of and remedies for failures in your products and materials. Our services Service Analysis of chemical composition and deformation Service Morphological study of materials Service Assessment of material failures: breakage, delamination, pollution, degradation, corrosion, adhesion, etc. Service Characterization of metal powders Service Characterization of PAH powders Service Surface analysis of materials: surface treatment, number of layers, deposition, surface finish Service Study of extractables and releasables from materials Service Nanomaterials analysis Service Extreme surface study The FILAB laboratory offers a physico-chemical analysis and characterization service for all types of materials. Characterization Metal alloys • Composition and deformation analysis Composition and deformation analysis Do you want to ensure the conformity of your metal alloys by studying alloys by studying their chemical composition? What's more, deformation techniques allow you to deepen your understanding of your alloys. understanding of your alloys. • Expertise on failures Expertise on failures Have metal alloy defects analyzed to understand their causes and consequences. We can carry out in-depth failure studies for you, to gain a better understanding of the nature and extent of defects. • Extreme surface study Extreme surface study The surface of a material is where all the interactions with its environment take place, potentially altering its performance and protection. Surface analysis refers to the analysis of a surface on a nanometric scale. • Impurity analysis Impurity analysis Analysis of impurities on a metal alloy: how can they affect performance? • On-site pollution analysis On-site pollution analysis Quickly analyze pollution on your metal parts with our state-of-the-art analytical equipment. Easily identify the nature of the pollution and take the necessary steps to remedy it. Characterization Polymers and composites • Extreme surface study Extreme surface study Get a nanoscale analysis to better understand the keys to materials performance and protection. • Dosing of hazardous substances Dosing of hazardous substances • Determination of molecular weight Determination of molecular weight • Polymer deformation Polymer deformation Discover what's inside your products with polymer deformation. This technique allows you to determine the nature and quantities of materials present in a formulation within a material. Reveal a product's true chemical composition with this in-depth analysis. • Analysis of chemical composition Analysis of chemical composition FILAB analyzes the chemical composition of metal alloys in the laboratory specific analyzers (C and O) and ICP. Characterization Surface analysis • Extreme surface study Extreme surface study The surface of a material is crucial to its interaction with the environment and performance and protection. Surface analysis at the nanoscale to understand the challenges your material faces. • Analysis of chemical composition Analysis of chemical composition • Morphological analysis Morphological analysis Explore the structure and layers of your samples with our analysis services, using light microscopy and scanning electron microscopy (SEM). Uncover hidden details and measure the thickness of individual layers. • Failure analysis Failure analysis Whether due to an internal manufacturing problem or a customer return, a product failure can have repercussions on its reliability, strength and performance. performance. Discover the reasons behind these failures and the consequences they entail. • Development and validation of surface treatment processes Development and validation of surface treatment processes FILAB offers technical and human solutions to help manufacturers detect and understand defects in organic or metallic processes. Don't let failure problems slow you down. Rely on our expertise. • Surface treatment analysis Surface treatment analysis Organic or metallic treatments can lead to failure problems over time, or due to poor compatibility with the product's environment. To detect and understand these defects, FILAB offers manufacturers its technical and human resources. Characterization Ceramic and glass • Analysis of ceramics and glass Analysis of ceramics and glass Our state-of-the-art analytical facilities at FILAB are capable of performing characterizations on ceramics and glass. • Analysis of chemical composition and deformation Analysis of chemical composition and deformation • Morphological study of materials Morphological study of materials Visual analysis of a sample using high-performance imaging techniques, such as microscopy or scanning electron microscopy (SEM). Thanks to these methods, you'll be able to better measure the thickness of the different layers present. • Crystallographic characterization Crystallographic characterization Optimize the performance of your materials by studying their atomic composition using XRD. • Determining physical properties Determining physical properties • Morphological and microstructural expertise and failure studies Morphological and microstructural expertise and failure studies Characterization Powders • Characterization of metal powders according to Ma-0015 Characterization of metal powders according to Ma-0015 Characterization of metal powders to Ma-0015 standard for additive manufacturing. • Characterization of PAH powders Characterization of PAH powders Analysis and characterization of your hydroxyapatite powders (HAP) carried out to ISO 13779-6 standard, by the FILAB laboratory. • Morphological study Morphological study Uncover a sample's hidden secrets with our advanced imaging techniques such as optical microscopy or scanning electron microscopy (SEM). As well as revealing relevant details, these methods also tell you about the thickness of the different layers present. • Purity control Purity control The quality of a powder will play a decisive role in improving its final results. That's why the FILAB laboratory carries out powder control analyses to support your manufacturing processes. • Characterization of organic powders Characterization of organic powders What analysis techniques can be used to characterize materials? The FILAB laboratory's analytical facilities cover 5 200m² and offer a range of techniques to best meet your material characterization needs. In addition, the laboratory invests heavily every year in its analytical facilities to maintain its high-performance technical resources. Our techniques Organic fraction analysis IRTF, GC-MS, HPLC Surface analysis SEM, AFM, TOF-SIMS, XPS Analysis of the mineral fraction ICP, SEO, XRD, Elemental analysers Thermal analysis ATG, Py-GCMS, DSC Other BET, Optical Microscope, Helium Pycnometry, GPC, DMA/TMA, Goniometer, Granulo Laser, IGA, ... Our FAQ What is material characterization technology? Materials characterization is a technique that has evolved over time. It became a formal field of scientific research at the beginning of the 20th century with the development of microscopy.It is an essential step in understanding their properties and performance. Numerous techniques are available to scientists and engineers to characterize a material, ranging from microscopy to spectroscopy.Materials characterization is a technique used to determine a material's chemical composition, crystalline structure, microstructure, morphology, mechanical and thermal properties... The choice of technique depends on the type of material to be characterized, the precision required and the information required. What tools are used to characterize materials? Some of the most commonly used tools for materials characterization include:microscopy (optical, electron, confocal, atomic force),spectroscopy (infrared, Raman, and other types of optical and radiation spectroscopy),X-ray diffraction,calorimetry,rheology,thermogravimetric analysis,and mass spectrometry. What is materials science? Materials science studies the structure, properties and performance of materials. It enables us to understand the relationship between a material's chemical composition, internal structure, physical properties, performance and applications.Materials science encompasses fields such as physics, chemistry, materials engineering and other related sciences. Materials scientists study a wide variety of materials, including metals, polymers, ceramics, composites and semiconductors. The aim is to develop new materials with improved properties, or to improve existing materials. What does materials chemistry consist of? Materials chemistry is the study of materials from a chemical point of view: structure, composition, reactions. It plays an essential role in the discovery and development of new materials.Analytical techniques used in materials chemistry include chemical synthesis and spectroscopy. But also advanced characterization techniques, such as X-ray diffraction, electron microscopy and nuclear magnetic resonance spectroscopy, to examine the properties of materials at the atomic scale.
Sectors of activity Metallurgy, Steelmaking and Foundry Analysis and Expertise Laboratory As a manufacturer, you are looking for a laboratory capable of carrying out metallurgy, steelmaking or foundry analysis. From the design to the market launch of a product with metal components, you will be faced with several types of problem, covering :Control of raw materialsSubstitution of metal alloysUnderstanding and anticipating the behavior of materials in their environment of usePerformance of surface treatmentsOptimizing manufacturing and machining processes to reduce the risk of failure.To help you solve these problems, the support of a reliable laboratory with high technical added value enables you to better understand the changes in the metallurgical sector, and to gain in efficiency in your activity. Nuclear Aeronautics Spatial Metallurgy Powders Steel industry Foundry Automotive Suppliers To help you solve these problems, the support of a reliable laboratory with high technical added value enables you to better understand the changes in the metallurgical sector, and to gain in efficiency in your activity. The FILAB laboratory supports manufacturers in metallurgy and steel analysis FILAB, a laboratory staffed by experts in metallurgy and steelmaking analysis and failure characterization, offers you analytical services from design to manufacturing and implementation of a product with metallic components. Backed by its experience and state-of-the-art analytical facilities, FILAB boasts a wide range of tools specific to the metallurgy sector, enabling it to provide the following services: Analysis Our metallurgy and steel analyses • Metal alloy grade control Metal alloy grade control The FILAB laboratory analyzes the chemical composition of metal alloys, mainly using specific and ICP analyzers. Discover our services • Surface analysis Surface analysis The surface of a material is crucial to its interaction and performance, and influences product reliability and strength. Knowing these properties helps to adapt manufacturing and treatment processes. Discover our services • Metal powder analysis Metal powder analysis Characterization of metal powders to Ma-0015 for additive manufacturing. additive manufacturing. • Hardness analysis Hardness analysis • Identification of an unknown alloy Identification of an unknown alloy Expertise Our expertise in metallurgy and steelmaking • Failure analysis Failure analysis The analysis of imperfections in your metal alloys enables us to determine their origins and impact. We carry out detailed failure analyses for an in-depth understanding of their nature and scope. • Microstructure study Microstructure study Understanding the microstructure of materials is crucial to the development and manufacture of a new product, or to the improvement of an existing product that shows new anomalies. Discover our services • Material/fluid compatibility study Material/fluid compatibility study Assessing the material compatibility between a container and its contents is essential to avoid pollution and related problems. • Metallographic examination Metallographic examination Laboratory metallography is the method used to analyze the structure of a metal alloy by examining it under an optical microscope (OM) following a dedicated preparation. • Training in analytical techniques Training in analytical techniques As an accredited training organization, FILAB supports your teams in learning new methods of analysis and characterization. Whatever your sector of activity, FILAB can support you in your analytical chemistry training. Discover our services Examples of standards applications Referential • Ma-0015 Standard • ISO5832-1, ISO5832-11, ISO5832-3, ISO5832-12 Standard • ASTM E 1447 • ASTM E 2594 • ASTM E 2371 Standard • NF EN 573-3 • NF EN 10088 • NF A 36-711 Standard • JSTD 001 Our technical resources Organic chemical analysis LC-ORBITRAP, GPC, RMN, IRTF Basic analysis techniques ICP-AES and ICP-MS Elementary analysis C/S, N/O, H Powder analysis DRX, MEB-FEG EDX, BET Spark Spectrometry SEO Surface analysis MEB-FEG EDX, XPS, TOF-SIMS Did you know? FILAB has numerous customer accreditations and approvals for the metalworking industry, including : ISO 17025 accreditation by COFRAC for physico-chemical analysis of metallic materials Approved by SAFRAN for metal powder analysis according to Ma-0015 criteria Approved by FRAMATOME on metal alloy analysis Les Filab Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure Contactez-nous Pour répondre à toutes ces prestations, n'hésitez pas à contacter notre équipe. Nous contacter +33 (0)3 80 52 32 05 Demander un devis
Our services Laboratory analysis of nanomaterials in line with the REACH regulation REACH & nanomaterials : The 1907/2006 REACH regulation has undergone various changes, and made the declaration of nanomaterials mandatory.From January 1st 2020 onwards, producers and importers of nanomaterials, nanoparticles and all other forms of nanotechnology have been required to declare their activities as part of the REACH regulation. Physicochemical data also needs to be provided.The 1907/2006 REACH regulation refers to the EC 2011 regulation for its definition of nanomaterials.  How can FILAB assist you in analyzing nanoparticles in accordance with the REACH regulation ? FILAB provides a compilation of services centered around nanomaterials and the REACH regulation. Our laboratory is equipped with many machines capable of characterizing nanomaterials following definitions and conditions defined by REACH. FILAB : 1st French laboratory to receive ISO 17025 accreditation for nanoparticle characterization!* MP nano classification (EC 2011), Review of existing analytical data, Generation of additional data on nanoparticle characteristics... FILAB provides reliable and timely services led by our experts:Chemical composition analysis of nanoparticle-based products and trace residue analysis (ICP-AES, ICP-MS)Nanoparticle size and shape determination by SEMCount and particle size distribution measurement by SEM, DLS, Laser GranulometryCharacterization of nanoparticles’ surfaces, Zeta Potential, TGA, SEM, FTIR, Raman, ToF-SIMS, XPSBET specific surface area measurement and Helium Pycnometry density measurementDevelopment and validation of analytical methods specific to nanomaterials found in food productsContainer/Contents interaction testingNanoparticle detection by SP-ICP-MS or A4F-ICP-MSLiterature and regulatory reviewsAnalytical training *The scope of our accreditation covers : Nanoparticle size and shape distribution using SEM-EDXNanoparticle size determination using SP-ICP-MS(Details available at www.cofrac.fr - accreditation n°1-1793) What is the REACH analysis for nanomaterials? The REACH analysis for nanomaterials aims to assess the potential risks that these materials may pose to human health and the environment. Under EU legislation, manufacturers and importers of nanomaterials must demonstrate the safety of these materials before they can be marketed. To do this, they must carry out a risk assessment and provide detailed information on the properties and uses of these materials.This is an important part of the regulatory process to ensure that these materials are used safely. Manufacturers and importers are required to provide clear and accurate information on the potential risks of nanomaterials, enabling users to make informed decisions about their use. Why is it necessary to refer to REACH for nanomaterials? It is essential to refer to REACH when analysing nanomaterials as this legislation regulates the production, import and use of many chemicals in Europe, including nanomaterials. This regulation establishes specific criteria for the assessment and management of risks associated with the use of nanomaterials, including data and testing requirements.By complying with REACH, manufacturers and importers of nanomaterials can demonstrate the safety of their products, contribute to the protection of human health and the environment, and ensure regulatory compliance. Users of nanomaterials can also be assured that the products they use meet the highest safety standards.
Our services Surface analysis and characterization laboratory Your needs: surface characterization of your materials Knowing the properties and surface conditions of a material can help you adapt your manufacturing processes. The support of a specialized laboratory will enable you to carry out analyses and expert appraisals on the surface of materials to optimize your performance.The surface of a material is a vulnerable zone where numerous interactions with its environment take place. Its specific characteristics determine the overall performance of materials. In the event of failure (corrosion, wear, adhesion, friction, etc.), it can have an impact on a product's reliability and durability. Nuclear Aeronautic Spatial Medical Electronic Defense/Security Automotive Our customized surface analysis services and techniques Analysis Our analysis services • Analysis of surface chemical composition Analysis of surface chemical composition Surface chemistry is concerned with the surface properties of materials. It enables us to modify the chemical properties of surface materials, if necessary, to give them new properties adapted to their utility. • Morphological and topographical study Morphological and topographical study Morphology, the three-dimensional study of surfaces, and topography, analyzed at macro, micro and nanometric levels, are crucial for optimizing industrial manufacturing processes. These analyses help prevent failures by providing an in-depth understanding of material properties. • Thickness measurement of surface layers Thickness measurement of surface layers Multilayer analysis of material surfaces involves examining several surface layers of a material. This technique is widely used to identify the surface composition of materials. • Control of surface cleanliness Control of surface cleanliness The surface of a material interacts with its external environment and may encounter chemical contamination or particle pollution as a result of the various stages in the manufacturing process, for example. Expertise Our expert services • Nanoscale surface analysis (extreme surface analysis) Nanoscale surface analysis (extreme surface analysis) FILAB is able to analyze the surface of a material on a nanometric scale (extreme surface analysis) using cutting-edge techniques such as TOF-SIMS, XPS/ESCA and AFM. • Identification of surface pollution Identification of surface pollution As well as checking the surface cleanliness of the material, the laboratory identifies the pollution in question. • Interface analysis Interface analysis Material interface analysis is a technique for studying the transition zone between two distinct substances in a composite material. It enables us to understand the chemical and physical interactions at interfaces, which are crucial to material performance and stability. • Failure study - characterization of a surface defect Failure study - characterization of a surface defect Corrosion, cracks, fractures, adhesion problemsBy analyzing the imperfections in your metal alloys, we can determine their origins and impact. We carry out detailed failure analyses to provide an in-depth understanding of their nature and scope. • Controlling the homogeneity of surface treatments Controlling the homogeneity of surface treatments Controlling the homogeneity of surface treatments is essential to ensure uniform material quality and performance, enabling any variations or defects in the treatment process to be detected and corrected. This verification guarantees the reliability and durability of materials in their specific applications. Research and development Our R&D services • Development and validation of treatment processes (functionalization or passivation) Development and validation of treatment processes (functionalization or passivation) The development and validation of surface treatment processes are fundamental to innovating and improving the performance of materials, by ensuring that each method is effective, reproducible and compliant with the required quality standards. This approach guarantees the reliability and effectiveness of the treatments applied, adapted to the specific features of each material. • Ageing study Ageing study Ageing studies enable us to predict durability and resistance over time. In particular, it enables us to anticipate changes in its properties under the effect of environmental and usage factors. • Support in choosing surface treatments Support in choosing surface treatments Surface treatments give materials a particular appearance and characteristics, depending not only on the type of surface treatment used, but also on the substrate on which the coating will be applied. • On-demand surface analysis training On-demand surface analysis training FILAB offers a range of training courses, but it is also possible to carry out training on demand. Our technical resources For over 30 years, the FILAB laboratory has had the experience and specific analytical equipment to meet the needs of surface analysis and characterization on all types of materials (metals, polymers, ceramics). FILAB offers the following surface analysis techniques: SEM-EDX read more + SEM-EBSD read more + AFM read more + ToF-SIMS read more + XPS read more + Our FAQ What is surface analysis? Surface analysis refers to a set of techniques used to study the physical, chemical and morphological properties of the surface of a solid material. This technique is widely used in materials science, physics, chemistry... What techniques are used for surface condition analysis? Techniques commonly used in surface analysis include scanning electron microscopy (SEM), atomic force microscopy (AFM), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction. These techniques provide information on the topography, chemical composition, molecular orientation and mechanical properties of a material's surface. When should a surface condition analysis be carried out? Surface analysis is particularly useful for understanding the properties and interactions of materials in applications such as catalysis, corrosion, friction, adhesion, electronics and many other areas of research and engineering. Les Filab Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure Contactez-nous Pour répondre à toutes ces prestations, n'hésitez pas à contacter notre équipe. Nous contacter +33 (0)3 80 52 32 05 Demander un devis
Our services Medical Device characterization in accordance with the ISO 10993-19 standard FILAB laboratory is able to assist you in characterizing your medical devices in accordance with the ISO 10993-19 standard The ISO 10993-19 standard provides a compilation of parameters and test methods that can be useful for the identification and evaluation of the physical, physicochemical, morphological and topographical (PMT) properties of materials in finished medical devices. PMT parameters play an important role in evaluating the biocompatibility and the clinical efficiency of medical devices.The ISO 10993-19 standard therefore states which properties are to be taken into consideration when characterizing the PMT parameters of materials containing polymers, metals, alloys, ceramics, and natural macromolecules.With support from a partner laboratory, FILAB is able to assist you in evaluating the biocompatibility of your Medical Devices by conducting the following tests : Our tests Chemical characterization in accordance with the ISO 10993-19 standard Degradation testing in accordance with the ISO 10993-13, ISO 10993-14 and ISO 10993-15 standards Chemical characterization in accordance with the ISO 10993-18 standard Nanomaterial characterization in accordance with the ISO 10993-22 standard  We are also able to provide the following services : Our services Cytotoxicity testing in accordance with the ISO 10993-5 standard Skin irritation testing in accordance with the ISO 10993-10 standard   Toxicological evaluations of leachable substances in accordance with the ISO 10993-17 standard The fact that we work on a human scale, our continuous investments and our extensive knowledge of the field of Medical Devices all ensure the reliability of our results, a quick turnaround for requests and tailored support suited to your needs. Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure Why choosing an ISO 10993-19 certified laboratory? Choosing an ISO 10993-19 certified laboratory is important for several reasons: Compliance with Regulatory Requirements: Regulatory agencies such as the European Medicines Agency (EMA) require medical device manufacturers to provide comprehensive data on the physico-chemical, morphological, and topographical characterization of materials used in their devices. Working with an ISO 10993-19 certified laboratory can help ensure that your testing meets these regulatory requirements. Expertise and Experience: An ISO 10993-19 certified laboratory has the expertise and experience necessary to conduct thorough material characterization testing. The lab personnel are trained in the specific techniques and methods required for these tests, and they have a deep understanding of the relevant regulations and guidelines. Quality Assurance: An ISO 10993-19 certified laboratory must adhere to stringent quality assurance and quality control standards. This means that the lab follows established protocols for sample preparation, testing, and data analysis, ensuring that the results are accurate, reproducible, and reliable. Risk Mitigation: Failure to adequately characterize the materials used in a medical device can lead to product recalls, safety issues, and legal liability. Choosing an ISO 10993-19 certified laboratory can help mitigate these risks by ensuring that your device materials are thoroughly tested and meet all applicable safety standards. What are the mandatory clauses of ISO 10993-19 to be met? ISO 10993-19 is a standard that provides guidance on the physico-chemical, morphological, and topographical characterization of materials used in medical devices. The standard outlines several mandatory clauses that must be met to ensure that materials are thoroughly characterized and safe for use in medical devices. These include: Sample Preparation: This clause outlines the requirements for preparing samples for testing, including the size, shape, and number of samples required. Identification of Materials: This clause requires the identification of all materials used in the device, including any additives or impurities that may be present. Physico-Chemical Properties: This section outlines the tests required to evaluate the physico-chemical properties of the materials, such as solubility, pH, and viscosity. Morphological and Topographical Characterization: This clause requires the evaluation of the morphology and topography of the materials, including their surface area, porosity, and roughness. Surface Properties: This clause outlines the requirements for evaluating the surface properties of the materials, including surface tension, contact angle, and surface energy. Chemical Characterization: This clause requires the identification and quantification of chemical substances present in the device, including any additives or impurities that may be introduced during the manufacturing process.Biological Evaluation: This clause requires manufacturers to conduct in vitro and/or in vivo biological evaluations to assess the biocompatibility of the materials. What are the main methods used for medical device characterization within ISO 10993-19? ISO 10993-19 outlines several methods for the characterization of materials used in medical devices. These methods can be broadly categorized into three groups: physico-chemical characterization, morphological characterization, and topographical characterization. Some of the main methods used in each of these areas include: Physico-Chemical Characterization:Fourier Transform Infrared (FTIR) SpectroscopyThermogravimetric Analysis (TGA)Differential Scanning Calorimetry (DSC)X-ray Photoelectron Spectroscopy (XPS)Atomic Absorption Spectroscopy (AAS)Inductively Coupled Plasma Mass Spectrometry (ICP-MS)Gas Chromatography-Mass Spectrometry (GC-MS) Morphological Characterization:Scanning Electron Microscopy (SEM)Transmission Electron Microscopy (TEM)Atomic Force Microscopy (AFM)Confocal Laser Scanning Microscopy (CLSM)Light Scattering TechniquesMechanical Profiling Topographical Characterization:Contact Angle GoniometrySurface Roughness MeasurementsScanning Probe Microscopy (SPM)Optical Profilometry Overall, these methods are used to evaluate various aspects of a material's properties, such as chemical composition, thermal stability, morphology, surface topography, and wettability. The results of these tests are critical for ensuring that the materials used in medical devices are safe, effective, and meet all regulatory requirements. 
Sectors of activity Laboratory analysis in line with GMPs Your needs : to call on an analytical laboratory working in a GMP environment providing various services for the pharmaceutical industry What are GMPs ? GMPs (good manufacturing practices) are defined by the WHO (world health organization) as “the aspect of quality assurance that ensures that medicinal products are consistently produced and controlled to the quality standards appropriate to their intended use and as required by the product specification”.In the pharmaceutical industry, GMPs are very important given the high level of quality that is required during the development, production and monitoring of products.GMPs cover the notion of quality assurance throughout the development, production and monitoring processes of pharmaceutical products and not just on the finished product.GMPs apply to pharmaceutical products intended for both human or animal consumption.For years, competent authorities have been looking to harmonize GMPs worldwideThe ICH Q7, Q8, Q9, Q10 can be fully integrated into GMPs on different levels, such as ICH Q7 which specifies the GMPs for active ingredients (API) or even ICH Q8, Q9 and Q10 which mention the “quality by design” approach for GMPs. What criteria does an analytical laboratory have to fulfil to fall in line with GMPs ? A laboratory working in accordance with GMPs must abide by certain guidelines :A location up to standardsTrained and qualified personnelQualified equipmentComplete traceability via a reliable registration systemProcedures written out and validated by quality assuranceA regular internal audit systemAre you looking to cooperate with a reliable and reactive analytical laboratory, working in line with GMPs and abiding by the above guidelines ? Call on FILAB ! Our solutions : to assist pharmaceutical industrialists with expertise services in line with GMPs At FILAB, we have been carrying out various analysis for the pharmaceutical industry in line with GMPs and regulations for many years. We have ISO 17025 accredited (www.cofrac.fr accreditation n°1-1793) for the analysis of elemental impurities in pharmaceutical matrices. Our clients regularly audit our laboratory in relation with GMPs.From analysis to expertise, FILAB laboratory is able to provide the following services for the pharmaceutical industry :Custom chemical analysis of pharmaceutical productsDetection of elemental impurities in accordance with the USP 223Expertise of pharmaceutical packaging materialsProblem solving (ICH Q3D)Analysis of residual solvents in accordance with the USP 467 (ICH Q3C)Analysis of nitrosamines in pharmaceutical productsAnalytical developmentAnalytical training and validation (ICH Q2)Forced degradation studies on pharmaceutical products or packagingStability testingDissolution testing Powder characterization and granulometric analysisExtractables and leachables testingAnalysis of particulate contaminates in injectable drugs Our facilities Organic analysis : GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIRMineral analysis : ICP, XRD, ICThermal analysis : TGA, DSGPowder analysis : XRD, SEM FEG EDX, BETSurface analysis : SEM-FEG EDX, XPS, ToF-SIMS Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Laboratory analysis of surface chemistry Analysis of surface chemistry, one of FILAB’s many skills Surface chemistry is the study of the surface properties of materials. Surface chemistry can be used to alter the chemical properties of surfaces to give them new properties better adapted to a material’s use. Surface chemistry can be used to analyze varnishes, coatings, specific industrial treatments, paints, etc. Our analytical techniques relating to surface chemistry FILAB laboratory is equipped with a cutting-edge analytical fleet and has extensive multisectoral expertise making it possible for us to reliably fulfil requests from industrial clients for surface chemistry analysis.Our laboratory is able to use multiple complementary analytical techniques such as :ToF-SIMSXPSOur competence and our dual expertise in chemistry and materials science ensures that our complete, reliable services will fulfil your needs for surface analysis. These techniques are complementary to our other means for surface analysis such as SEM FEG EDX or Optical Microscopy. Examples of problems resolved by the analysis of surface chemistry In the medical field :Surface cleanliness assessment of a Medical Device as part of the validation process for a cleaning procedureIdentification of residual detergents on the surface of an implant with the use of complementary techniques such as ToF-SIMS and XPSCharacterization of the surface of a Medical Device : morphology by FESEM, elemental surface analysis by XPS, molecular characterization by ToF-SIMS, detection of contaminants…Aeronautics/Automobiles :Assessment of an adhesive problem when painting a material (elemental identification of a pollutant by XPS or FESEM, molecular analysis by ToF-SIMS…)Identification of sizing agent found on the surface of fibers used to make composite materialsCharacterization of a passivation procedure for aluminum alloy Electronics :Identification of a pollution present at the interface of an assembly causing an adhesive problemFailure analysis following a loss in performance Pharmaceuticals :Identification of contaminants found on the interior surface of glass bottlesOutermost layer characterization of packaging displaying sealing problems Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Laboratory analysis of nanomaterials and nanoparticles for the food industry Reminder : what does the INCO 1169/2011 regulation state regarding the use of nanomaterials in the food industry ? In the food industry, the use of nanomaterials is becoming more and more widespread, especially in packaging where silver nanoparticles can be used for their antibacterial properties. Other nanoparticles such as Titanium dioxide (TiO2), Silicon dioxide (SiO2) or even Iron oxide are used in food products to improve texture, color or eve, viscosity. Used as dyes, thickeners or preservatives, TiO2, SiO2 and Fe2O3 are better known as food additives E551, E171 and E172 respectively.However, the impact of this new technology is having on human and environmental health is still unknown. Many studies have shown the adverse effects nanoparticles cab have on the human body when inhaled or ingested. Because of this it is essential to declare the presence of nanoparticles being produced, used and distributed to ensure their traceability. (“R-Nano” declaration in France). FILAB can assist you in inspecting nanoparticles found in your packaging or food products FILAB  : 1st French laboratory to receive ISO 17025 accreditation for nanoparticle characterization!* FILAB provides a compilation of services centered around nanomaterials, namely those that can be found in the food industry. Our laboratory is equipped with many machines capable of characterizing nanomaterials.Relying on our experts, FILAB is able to provide the following services :Detection of nanoparticles and nanomaterials in food products or packagingNanometric classification of raw materials and finished productsChemical composition analysis of nanoparticle-based products and trace residue analysis (ICP-AES, ICP-MS)Nanoparticle size and shape determination by SEMCount and particle size distribution measurement by SEM, DLS, Laser GranulometryCharacterization of nanoparticles’ surfaces, Zeta Potential, ATG, SEM, FTIR, Raman, ToF-SIMS, XPSBET specific surface area measurement and Helium Pycnometry density measurementDevelopment and validation of analytical methods specific to nanomaterials found in food productsContainer/Contents interaction testingNanoparticle detection by SP-ICP-MS or A4F-ICP-MSLiterature and regulatory reviewsAnalytical training*Our accreditation scope covers : Nanoparticle size and shape distribution using SEM-EDXNanoparticle size determination using SP-ICP-MS(Details available at www.cofrac.fr - accreditation n°1-1793) Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Surface treatments : coating thickness measurements Material surfaces are subject to numerous interactions with their environment. To add a specific functionality needed to meet the requirements of a given application, surface treatments are used to change the appearance of a material (decoration, luxury…), as well as its physicochemical properties : resistance to corrosion and wear, optical properties… Surface treatments : coating thickness measurements Contrary to conversion and thermochemical treatments, surface treatments consist in adding a thin layer, rarely thicker than a millimeter and can even be only a few nanometers thick. These deposits usually fall into two categories :Wet deposits, such as electrolytic deposits, chemical deposits (nickel, copper…) and immersion deposits (galvanization, tin plating…)Dry deposits, such as thermal projections, vapor deposits (CVD and PVD), plasma assisted deposits… Other techniques for coating thickness measurements​ Inspecting coating thickness is a key step to ensure the functionality of a surface treatment. This can be done non-destructively (Eddy current, Ultrasound, X-ray fluorescence…) this measurement is also implemented after specific cross section preparation (coating and polishing, localized ion-beam, microtomy…) using different characterization techniques :Optical microscopy (binocular, metallographic microscopy…)Conventional scanning electron microscopy (SEM) or with a field emission gun (FEG) usually paired with a microprobe (Energy Dispersive Spectroscopy) used to determine the elemental chemical composition of a surface treatment Transmission Electron Microscopy (TEM) on a thin slide to access nanometer thick layersOther more complex analytical techniques such as X-ray Photoelectron Spectroscopy (XPS), Secondary Ion Mass Spectrometry (SIMS) or Glow Discharge Mass Spectrometry (GDMS) can also be used. Why choose FILAB laboratory for the coating thickness measurement ? With extensive experience in implementing these different techniques and having renown expert knowledge, FILAB is able to assist you with analysis and inspections of coating thickness and of defects found in the surface treatment.For more information, feel free to contact us via email at contact@filab.fr
Our services Laboratory analysis of metals FILAB laboratory provides metallographic examination services as well as chemical analysis services for your metals. Our cutting-edge analytical fleet allows us to analyze both ferrous and non-ferrous metals. Your needs : to analyze your metals To assess the reliability and the compliance of your metal parts, you need to carry out testing on your metals. The analysis of metal samples is a key step both in a regulatory context but also to avoid the appearance  of defects during the production process. Our solution : to provide expert analysis services for your metals FILAB laboratory has been specialized in analyzing metals for over 30 years, providing mechanical testing and metallographic examinations. We are equipped with cutting-edge equipment for the analysis of your metals and to fulfil your requests regarding metals, FILAB laboratory is able to offer the following services : our solutions Compositional analysis of metals by ICP (ICP-AES, ICP-MS and ICP-MS/MS) and using an elemental analyzer Micro-structural analysis by SEM-EDX Outermost surface layer analysis by SIMS or XPS Metallographic analysis Failure analysis : corrosion, ruptures… Surface analysis by FTIR or TGA-FTIR Mechanical testing Strength testing Thanks to a high level of technical skill and a cutting-edge analytical fleet, FILAB laboratory is able to ensure quick and reliable services and for the analysis of metals with ISO 17025 accreditation.Feel free to contact our department dedicated to metallic analysis via email at contact@filab.fr or over the phone by +33 (0)3 80 52 32 05. Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Sectors of activity Microelectronics analysis in a laboratory Yours needs: to manufacture performant and adapted microelectronics For the past fifty years, the microelectronics industry has been tremendously used in the science and research fields but also in several day-to-day items.In several fields such as aeronautics, spatial, defense and medicine, manufacturing smaller and smaller components is a way to innovation and efficiency.In light of this, the analytical methods and techniques used so far must be increasingly precise and efficient.As major microelectronics manufacturer for high-tech use or subcontractor in micro-technology, you need to :Analyze your raw materialsControl the cleaning processVerify the compliance of the surface treatmentCharacterize any production defect Our solutions: to provide you with our skills and our analytical tools and adapting them to your microelectronics related challenges With an analytical fleet spread over 5 200m² and a team made up of doctors and engineers, FILAB can assist industrialists in analyzing and characterizing their microelectronics.To overcome these specific challenges with precise and reliable results, FILAB offers a wide range of analytical techniques : Our services Thermal analysis Polymer analysis Composite materials analysis Powder analysis Surface analysis Chemical analysis (heavy metals, additives, residual solvents...) Metals analysis Granulometric analysis REACH analysis Expertise Chemical expertise Deformulation analysis Nanomaterial characterization Compatibility study (interactions container/content, chemical releasing...) We also help you with: Bibliographic reviews Analytical development  Audits Process optimization Customized training courses Validation of new methods Our means Organic chemical analysis : HS-GC, Py-GCMS, LCMS/MS, SEC, NMR, FTIR Mineral chemical analysis : ICP, XRD, IC Thermal analysis : TGA, DSC Metallurgical analysis : ICP, SEM, SEO Powder analysis : XRD, SEM, BET Surface analysis :SEM, XPS, TOF-SIMS Contact us Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Analysis and polymer testing in a laboratory You need to determine the different components in a unknown or partially known polymer? You are facing difficulties due to polymerization? You need a lab to analyze and help you understand why your polymer doesn't work as it should? FILAB laboratory realise polymer testing analysis. Because of the wide range of testing equipment available within FILAB, we are able to carry out a full set of polymer tests to provide you with a comprehensive evaluation of your samples including to characterize trace impurities and measure unknowns. Polymer testing analysis To analyze and characterize your polymers, we use several methods such as: FTIR to identify the nature of a polymer HS-GC to identify the different additives and monomers ICP to identify mineral products We can also quantify the impurities in you polymers On the other hand, we can also help you quantify and characterize any pollution in your products. To do so, we start with analyzing your products, then we adapt our methods to your needs : SEM/EDX to analyze the particules, HS-GC for organic molecules such as phtalates, plasticizing agents, solvents… ICP/MS for heavy metals DSC for polymerization kinetic study, to optimize the polymerization process and check the catalytic performance of your polymer For over 20 years, FILAB laboratory has had the experience and the specific analytical fleet to be able to assist industrial companies with analysis and polymer testing all while providing tailored support. Contact us ! Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure In which context might you need to perform polymer testing ? Polymer analysis and characterization is used in a wide range of contexts, from research and development to quality control and failure analysis. Here are some common contexts where polymer testing may be needed: Research and Development: Polymer characterization is often used to evaluate the properties and behavior of new polymer materials, such as their molecular weight, thermal properties, mechanical properties, and chemical structure. This information can be used to develop new products or improve existing ones. Quality Control: Polymer testing can be used to ensure that polymer materials meet certain specifications and standards, such as those related to performance, safety, and environmental regulations. This includes testing for properties such as tensile strength, elongation, and hardness. Failure Analysis: Polymer testing can help identify the root cause of a failure in a polymer component or product. By examining the chemical and physical properties of the material, researchers can determine if the failure was caused by a defect in the material itself or by other factors such as processing conditions or environmental exposure. Regulatory Compliance: Polymer characterization may be required to meet regulatory requirements, such as those related to food contact materials, medical devices, and other consumer products. This includes testing for properties such as biocompatibility, migration, and toxicity. Process Optimization: Polymer testing can be used to optimize production processes, such as extrusion, injection molding, or blow molding. By understanding the properties of the polymer material, researchers can adjust the process conditions to achieve the desired physical and chemical properties. Overall, characterization of polymers is a critical tool for understanding and optimizing polymer materials and products in a wide range of contexts. Which industries might need the services of a polymer testing lab ? Polymer testing is an essential tool used by many industries to ensure the quality and performance of polymer materials and products. With its ability to examine the chemical and physical properties of polymers, polymer testing can provide invaluable insights into the behavior of polymer materials in different applications. Find out about the key industries that may need the services of a polymer testinglab, and how polymer characterization can help them achieve their goals. The Plastics and Polymers Industry The plastics and polymers industry is one of the largest users of polymer characterization services. Polymer testing is used extensively in the development and production of plastic products, such as packaging materials, automotive components, and medical devices. By understanding the properties of polymers, manufacturers can optimize their production processes, reduce waste, and ensure that their products meet the required standards for performance and safety. Medical Devices Polymer testing is essential to ensuring the safety and efficacy of medical devices made from polymers. Medical devices such as catheters, implants, and drug delivery systems require precise characterization to ensure that they are biocompatible, non-toxic, and effective in their intended use. Aerospace Aerospace applications such as structural composites, thermal insulation, and adhesives require precise characterization for their effective implementation. Polymer testing can help aerospace manufacturers develop materials that are lightweight, strong, and resistant to extreme conditions. The characterization of polymers by a specialized laboratory helps industries ensure quality and performance. Other sectors such as construction materials, electronics, automotive and textiles might also regularly require it. Overall, polymer characterization is a crucial tool for many industries that use or produce polymer materials. By working with a polymer characterization lab, these industries can ensure the quality, safety, and performance of their products, and optimize their production processes for maximum efficiency and effectiveness. What is polymer surface characterization ? Polymer surface characterization refers to the process of analyzing and understanding the chemical and physical properties of the surface of polymer materials. The surface characteristics of a polymer can play a significant role in its performance, function, and interactions with other materials. Surface characterization allows researchers to study the topography, chemistry, and morphology of the surface at a microscopic level. The surface of a polymer material is typically different from its bulk properties, due to factors such as molecular orientation, surface roughness, and the presence of additives and contaminants. Polymer surface characterization techniques aim to provide detailed information about these differences, which can help researchers understand the behavior of the material in specific applications. Common techniques for polymer surface characterization include: Scanning electron microscopy (SEM): This technique uses a focused beam of electrons to produce high-resolution images of the surface of a polymer material. SEM can be used to study the surface morphology, topography, and microstructure of the material. Fourier-transform infrared spectroscopy (FTIR): This technique uses infrared radiation to measure the absorption or transmission of light by the polymer material. FTIR can be used to study the chemical composition of the polymer surface. X-ray photoelectron spectroscopy (XPS): This technique uses X-rays to excite electrons in the polymer material, which are then detected and analyzed. XPS can be used to study the chemical composition and bonding of the polymer surface. Atomic force microscopy (AFM): This technique uses a sharp probe to scan the surface of the polymer material and produce a high-resolution image. AFM can be used to study the surface topography and mechanical properties of the material. Contact angle measurement: This technique involves measuring the angle between the surface of a droplet of liquid and the surface of the polymer material. Contact angle measurement can provide information about the wettability and surface energy of the material.
Sectors of activity Characterization of the passivation of medical devices Your needs: check the corrosion resistance performance of your implants What is a passivation process? Passivation is a chemical process that consists of treating the surface of a metal alloy in order to cover it with a uniform and compact layer of oxides thus improving its resistance to corrosion by acting as a barrier against external aggressive elements. Why characterize the passivation of medical devices? The surfaces of implants are the preferred sites for interactions with the biological host environments. In order to avoid adverse effects after deployment in the human body, medical devices must therefore have excellent corrosion resistance. Optimizing the corrosion resistance of medical devices is therefore essential for the biomedical field. Therefore, the FDA requires supporting data to demonstrate that a medical device has sufficient corrosion resistance. Thus, controls must be carried out in order to verify the integrity and the thickness of the treatments, the conformity of the specifications, the corrosion resistance performance, ... Our solutions: characterize your passivation treatments and evaluate their performance Our laboratory services to evaluate passivation processes For more than 30 years, our FILAB laboratory has had the know-how and complementary state-of-the-art analytical equipment to support manufacturers in the medical device sector in the characterization of passivation treatments, both in the context of control and in the framework of failure assessment and process optimization. The FILAB laboratory thus offers a multisectoral expertise in the face of several types of requests related to the passivation of medical devices: Characterization of the metallic and oxide forms of the chemical elements present on the surface of a medical device Observation of the uniformity and integrity of a surface treatment Measurement of the passivation thickness of a medical device Corrosion resistance test (salt spray test, ...) Expertise of a corrosion initiation observed on a passivated device Support for the optimization of a passivation process of a metallic implant in titanium alloy or stainless steel. For this type of service, the FILAB laboratory uses state-of-the-art analysis techniques such as Scanning Electron Microscopy coupled with a microprobe (SEM FEG-EDX), X-ray Photoelectron Spectroscopy (XPS) associated with corrosion tests (salt fog chamber) or even elementary analysis techniques (ICP-AES, ICP-AES, CLI)
Sectors of activity MEDICAL DEVICES : problematic adhesion of PAH on femoral head Faced with major strategic and regulatory challenges, the medical device sector is growing rapidly in France and Europe. Ensuring the quality of finished products, verifying the biocompatibility of the materials used, optimizing your processes and cleaning procedures, testing the endurance and stability of your items in specific environments, etc.: these are all daily issues for which the players in the medical device market must provide answers! Nowadays, the materials used for medical devices are multiple: metallic alloys (stainless steel, titanium, chrome-cobalt), organic materials (PEEK), ceramics, ... Their success is mainly based on their excellent mechanical properties, biocompatibility and corrosion resistance. Used for many years to promote tissue repair and osseointegration, bio-active ceramics are now widely used in the medical device sector. Hydroxyapatite (or HAP) is one of the most sought-after ceramics when applied by projection as a coating on orthopaedic implants. It is in this context that one of the main actors of PAH plasma spraying requested our laboratory to understand the origin of an adhesion defect of this type of coating on a metallic substrate revealed during production control tests. The expertise proposed by our laboratory consisted first of all in characterizing from a morphological point of view by Field Effect Scanning Electron Microscopy (FEG-SEM) the decohesive surface between the coating and the substrate. Chemical analysis techniques such as X-ray Photoelectron Spectroscopy (XPS) and Secondary Ion Mass Spectrometry (SIMS) were then used to highlight the potential presence of surface pollution at this failure interface. The results made it possible to rule out a possible origin of the problem associated with the spraying process and to carry out specific actions upstream of this process which made it possible to eliminate the defect. Thanks to the human skills and the complementary technical means available in our laboratory, FILAB was able to support this industrialist both from a technical point of view within the framework of the characterization of his defect and from a consulting point of view in order to solve his problem. With significant experience in the implementation of these adhesion defect expertises, FILAB can assist you in the context of your problems associated with the medical device sector. Download our Medical Devices brochure FILAB can also assist you with the following services:  Biocompatibility studies according to ISO 10993 ( -18 / -12 / -13 / -14 / -15 / -19 / -22 ) R&D support: custom chemical analysis, material and surface characterization, analytical development Problem solving: non-conformity, breakage, adhesion, corrosion...   Process validation: Cleaning (ISO 19227), surface treatment For more information, contact our expert: contact@filab.fr
Our services Identification of a foreign body in the laboratory You are looking to analyze a foreign body found in a product or on an industrial process ?  Throughout the manufacturing or marketing process of a product, there are many sources of contamination that can lead to the appearance of foreign bodies. The foreign bodies can be of several natures: organic, mineral or metallic.The presence of foreign bodies can deteriorate the performance of the product or the process; therefore, the identification of this foreign body with the support of a specialized laboratory is an essential step, especially if the foreign bodies are invisible to the naked eye.  FILAB supports manufacturers in the identification and analysis of foreign bodies FILAB offers industrial companies high-level human skills and state-of-the-art analytical equipment in order to provide them with services that meet their quality and compliance criteria. In order to respond quickly and reliably to these problems (emergency package possible), FILAB offers tailor-made support for the identification and analysis of foreign bodies:Characterization of a foreign body by SEM-FEG-EDX, FTIR, GCMS, Optical Miscroscope...Search for a trace of a specific component (packaging, cleaning residues, equipment...).Purity analysis of a raw materialSearch for impurities (ICH Q3D context) in pharmaceutical productsAnalysis of particles and contaminants Assistance in the creation of a defect libraryProcess audit Request a quote Technical means associated with the identification of foreign bodies : Organic chemical analysis: GCMS, Py-GCMS, LC-MSMS, LC-QTOF-MS, GPC, NMR, FTIR, RAMANInorganic chemical analysis: ICP, CISurface analysis: SEM-FEG EDX, XPS, TOF-SIMS Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Laboratory for failure analysis in the glass industry Failed materials in the glass industry: beware of breakage! What are the problems faced by manufacturers in the glass sector? The glass industry is one of the few sectors whose manufacturing techniques are essentially based on craftsmanship. The non-standardization of production tools, the fragility of materials and the scarcity of know-how give the glass industry strong industrial constraints in the design of solid, innovative glass that respects health and environmental requirements.Flat glass, hollow glass, fiberglass or crystal, the study of their characteristics will allow companies to better control their assembly, packaging and use. This technical challenge leads manufacturers and distributors in the glass sector to call upon service providers to assist them in controlling their materials, optimizing their production process and developing effective surface treatments. The FILAB laboratory is generally solicited for two types of problems - Interactions between the packaging and its environment (appearance of an external deposit or stain, wear, oxidation, etc.) - Interactions between the packaging and its contents (migration phenomenon) In the first case, the failure generally occurs after the product has been placed on the market, alerted by customer complaints, for example, requiring a high level of reactivity in the handling of analysis. At FILAB, the investigation of this failure is built in a methodical way: 1.characterize the chemical composition of the deposit by SEM-FEG-EDX, XPS, TOF-SIMS, ICP-MS or GC-MS according to its nature (organic, mineral) 2.identify the origin of the deposit: verification of the conformity of the packaging, surface characterization, audit of the production process... 3.provide a detailed expertise and propose adapted solutions to avoid again the risks of failures: determination of the root cause, implementation of corrective and preventive actions, improvement of industrial processes, development of protective surface treatments of the packaging...  Concerning the second problem, the health issues are more important. Indeed, the possible migrations between the glass packaging and its contents can present risks for the consumer or the final user. To analyze and anticipate these phenomena, FILAB performs aging tests and then analyzes the chemical behavior of the substances present by ICP-AES or ICP-MS. The analysis results and their interpretation allow our customers to assess the risks and chemical compatibility between the packaging material - in this case, glass - and its contents. Both manufacturers and customers must therefore be vigilant in their manufacturing process in order to avoid failures related to the quality of the packaging or its use. Thus, controls upstream and downstream of the marketing will contribute to the quality of the final product. "Glass" to infinity and beyond with FILAB For many years, our laboratory has been offering its know-how in understanding and solving the problems of the glass industry. Our human and technical complementarity is a real asset for glass manufacturers.Mineral chemistry, material chemistry, organic chemistry, so many skills requested by the glass industry and gathered today in a single place in our laboratory, guaranteeing reactivity, confidentiality and performance.More than an analytical laboratory, FILAB supports you in all your R&D projects and industrial challenges in order to meet the evolutions of your sector.
Our services Copolymer Materials Analysis Laboratory Your needs: validate the quality and performance of your copolymers A copolymer is a polymer resulting from the copolymerization of at least two types of monomers. It is therefore formed of at least two repeating units. Copolymers have physico-chemical and mechanical properties that are intermediate to those obtained from polymers alone. However, faced with these even more complex structures, the chemical analysis and characterization of copolymers becomes an important step in the control of their transformation and the prediction of possible failures. Plastics manufacturers, raw material producers, processors, finished product manufacturers, you are looking for the skills of a reliable analytical laboratory with high technical added value for the analysis and characterization of your copolymer materials. Our solutions: support you in the analysis and characterization of your copolymers. By combining specific analytical tools for polymers and copolymers with reliable and accurate scientific interpretations, FILAB laboratory assists manufacturers in optimizing their manufacturing processes, in the search for substitute materials and in solving failure problems on copolymer materials.With a strong experience in the analysis of copolymers and a large analytical park, FILAB offers the following services Characterization of copolymers: study of physicochemical and thermal properties by DSC, ATG, ATG-FTIR, GPC, NMR, SEM and FTIRCustom chemical analysis to determine the components of a copolymer: search for additives by GC-MS, Py-GCMS, LCMSMS, CI...Deformation of copolymersDetermination of the molecular structure by GPCCompatibility study between copolymer materials and fluidsAnalytical development related to the dosage of additives in copolymers OUR RESOURCES Organic chemical analysis: GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIRInorganic chemical analysis: ICP, XRD, ICThermal analysis : ATG, DSCPowder analysis : XRD, SEM-FEG EDX, BETSurface analysis: SEM-FEG EDX, XPS, TOF-SIMSThese thermal analysis and physico-chemical characterization techniques are adapted to a large panel of copolymer materials, and allow to better know the performances and the quality of copolymer materials. Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Analysis laboratory according to the R-Nano regulation What is the R-Nano declaration? Since January 1, 2013, the date of entry into force of Decree No. 2012-232 of February 17, 2012, French manufacturers, importers or distributors of a substance, mixture or material in a nanoparticulate state (quantity greater than 100 grams/year) are subject to a declaration of use, as well as the obligation to provide physico-chemical data on them. The objective of this decree is to ensure the traceability of the use of nanomaterials in order to have a better knowledge of the market and of the volumes commercialized, and to be able to set up effective actions if the evolution of knowledge on the risks related to the use of nanoparticles/nanomaterials were to grow strongly. How does FILAB support you in the classification of nanomaterials for the R-NANO declaration? FILAB offers a range of services based on nanomaterials and in particular on R-NANO. Our laboratories are equipped with a wide range of technologies for the characterization of nanomaterials.FILAB supports you on : - MP nano classification (CE2011)- Review of existing analytical data- Generation of additional data on nanoparticle characteristicsOur nanomaterial analysis services: Chemical analysis of nanoparticle-based product composition and trace analysis (ICP-AES, ICP-MS)Determination of the size and shape of nanoparticles by SEMCounting and particle size distribution by SEM, DLS, Laser particle size analysisSurface characterization of nanoparticles and/or coated nanoparticles, Zeta potential, ATG, SEM, FTIR, Raman, Tof-SIMS or XPSSpecific surface measurement by BET and density measurement by Helium PycnometryDevelopment and validation of analytical methods specific to nanomaterialsTesting of container/content interactionsDetection and analysis of nanoparticles by SP-ICP-MS and A4F-ICPMSBibliographic and regulatory study on nanomaterialsTraining on nanomaterials*Our scope of accreditation includes :  Size and shape distribution of nanoparticles by SEM-EDXSize determination of nanoparticles by SP-ICPMS(More information on www.cofrac.fr - accreditation n°1-1793) Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Laboratory for the analysis of surface defects on metal parts As an industrialist you wish to carry out a surface defect analysis on a metal part The surface of a material is the seat of many interactions with its environment and conditions, by its specific characteristics, the performance and protection of materials.The analysis of a surface defect of a metallic part can answer several physico-chemical problems:In the case of an expertise to know the origin of a failure (corrosion, crack, adhesion problem, unknown pollution...)To optimize your manufacturing processes (surface treatment, machine parameters...) and improve the performance of your materials.To control the quality of the surface condition of materials Surface defect analysis on metal parts: a specific expertise of FILAB laboratory FILAB laboratory has state-of-the-art analytical equipment and multi-sector expertise enabling it to respond with high reactivity and reliability to the chemical analysis needs of its industrial clients for surface defects.Our laboratory provides several complementary analytical techniques such as :TOF-SIMSXPS/ESCAAFMOur skills and our complementarity in chemistry and materials assure you a complete and reliable expertise for all your needs of surface defect analysis. These techniques complement other surface analysis equipment such as SEM-FEG-EDX or our Optical Microscopes.  Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Laboratory for surface cleanliness analysis by Scanning Electron Microscope (SEM) Your needs: control the level of surface cleanliness of a product For many application sectors (medical, energy, aeronautics, automotive, electronics, ...), the lifespan and functionality of a product are directly linked to the level of chemical contamination and particulate pollution present on the surface following the various stages of the manufacturing process.In order to guarantee the surface cleanliness of a product and therefore its quality, it is therefore essential to set up a cleaning program specific to the substances used in the manufacturing process of the article.To evaluate the cleanliness of a surface, the preferred technique is that of Scanning Electron Microscopy (SEM-FEG) coupled with an EDX microprobe. This approach has the advantage of being able to map the spatial distribution of contaminants on the surface of the part. FILAB provides you with a state-of-the-art SEM-FEG-EDX to evaluate your surface properties From analysis to R&D, including expertise and validation of cleaning processes, the FILAB laboratory offers a multi-sectoral expertise for several types of requests related to the surface cleanliness of materials: Our expertise Particle and chemical mapping by SEM-FEG-EDX of the surface of aerospace components (metallic and ceramic) following a customer methodology transposed and validated in our laboratory Analysis of the particulate cleanliness of turned parts for the aeronautical and automotive sectors according to ISO 16232 and VDA19 standards Particulate contamination in injectable products and parenteral infusions (USP 788, PE 2.9.19 method 2, ...) Control of the surface condition by SEM-FEG-EDX of dental implants after treatment to search for organic contamination and residues of surface treatment such as blasting, sandblasting, ... (Clean Implant) Particulate contamination and chemical characterization of medical devices according to ISO 10993, ISO 19227 Identification of the nature of particles by SEM-FEG-EDX and FTIR microscopy in pharmaceutical solutions. Other analytical techniques can be used to evaluate the cleanliness of a surface such as µ-IRTF, X-ray Photoelectron Spectroscopy (XPS) and Time of Flight Secondary Ion Mass Spectrometry (ToF-SIMS), Chromatography techniques (GC-FID, GCMS, LCMS, ...), elemental analysis (ICP-AES, ICP-MS, CLI)...  Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our technical resources Laboratory of surface analysis by Scanning Electron Microscope (SEM) The FILAB laboratory performs surface analysis by Scanning Electron Microscopy (SEM) The surface of a material being exposed to the external environment is often more vulnerable than the rest of the material. In case of corrosion, wear, adhesion or friction it can deteriorate and impact the reliability of the product.The analysis of a material's surface, especially by SEM, allows you to adapt your manufacturing processes as well as the implementation of surface treatment or cleaning processes. The support of a laboratory specialized in surface analysis will provide you with the expertise and the analysis tools to carry out your controls. SEM surface analysis: a specific expertise of the FILAB laboratory For more than 30 years, FILAB has had the experience and specific analytical equipment to meet the need for surface and extreme surface analysis, particularly by SEM, on all types of materials (metallic, polymer, ceramic). Thanks to a tailor-made support, FILAB laboratory analysis your industrial problems related to surface analysis and advises you until the interpretation of the results.Analysis of the chemical composition of the surface by SEM-FEG-EDX, XPS or TOF-SIMSAnalysis and characterization of surface treatment by SEM-FEG-EDXMorphological study of the surface of a material (porosity, roughness,...) by SEM-FEG-EDXIdentification of surface pollution (analysis of particles, deposits,...) by SEM-FEG-EDXMeasurement of the thickness of surface layers by SEM-FEG-EDXCharacterization of the surface coating by SEM-FEG-EDXStudy of failures and surface defects by SEM-FEG-EDX (cracking, breakage, migration, corrosion...)Through our three levels of services - analysis, expertise and R&D support - FILAB assists companies of all sectors and sizes in solving their industrial problems, by providing its clients with the know-how and experience of its team. 
Our services Scanning electron microscopy (SEM-EDX) deposit analysis laboratory The FILAB laboratory performs SEM-EDX analysis of deposits In the context of your production process, or in the application environment of your products, you have identified an unknown deposit whose chemical nature and origin you wish to know. This deposit can be of different natures: mineral, metallic or organic. The SEM-EDX analysis will allow you to conclude on the chemical nature of your deposit. Deposit and contamination analysis: a specific department of the FILAB laboratory For more than 30 years, FILAB has had the experience and specific analytical equipment to meet the needs of deposit or pollution analysis in your products. Thanks to a tailor-made support, FILAB laboratory analyzes your problems and guides you until the interpretation of the results through the following expertise services:Characterization of a deposit or unknown pollution by SEM-EDX, FTIR, GCMS, XRD, ICP, µ-IRTF... Analysis of particles or particulate contaminants by SEM-EDX on the surface of materials or in a substanceProcess audit following the appearance of unknown deposits or pollutionExtreme surface analysis by TOF-SIMS or XPS
Our services Laboratory analysis of polymethacrylates (PMMA) Use of polymethacrylates (PMMA) in industry Polymethacrylates are transparent and resistant thermoplastics whose monomer is methyl methacrylate (MMA). Known as Plexiglas (registered trademark), polymethacrylate is used in the industry for the production of advertising signs, glass, prostheses and implants, optical fibers, battery kit ...  FILAB studies the chemical and thermal properties of PPMA Thanks to a dedicated polymer analysis laboratory, the FILAB laboratory assists industrialists in the study of the chemical, thermal and physical properties of polymethacrylate (PMMA) based materials: Deformation and study of the chemical composition of PMMAStudy of the thermal properties of PMMAExpertise following a problem: degradation, color change, odor, adhesion ...Study of compatibility between PPMA and a fluid FILAB's analytical park dedicated to polymer analysis Organic chemical analysis: GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Thermal analysis: ATG, DSC, Py-GCMS, ATG/FTIR Powder analysis: XRD, SEM-FEG EDX, BET, Laser granulometer Inorganic chemical analysis: ICP, XRD, CI Metallurgical analysis: ICP, MEB-FEG EDX, SEO Surface analysis: SEM-FEG EDX, XPS, TOF-SIMS, AFM
Sectors of activity Particle counting laboratory according to the AAMI TIR42 standard Medical device professionals, you want to analyze them according to the AAMI TIR42? What is AAMI ? First, AAMI develops standards for counting particulate contamination in Medical Devices. The AAMI Technical Information Report (TIR) addresses vascular exposure to particulate matter resulting from the manufacturing environment and use of medical devices.This TIR has several objectives to assist manufacturers of vascular medical devices, as follows: Determine the source of the particulate matter,establish product particle limits,define appropriate test methods, andassess the clinical relevance of particulate contamination. COFRAC ISO 17025 accredited, how does FILAB support you in particle counting analysis according to AAMI TIR42? FILAB is able to assist you in the analysis of particle counts according to AAMI TIR42. Indeed, the laboratory offers to industrialists specialized in the manufacture of medical devices technical skills and a state-of-the-art analytical park.The aim of this equipment is to respond in the best possible way and in a reactive manner to their request and to offer them the most appropriate services and a tailor-made follow-up. It is also possible to perform these analysis on an emergency basis.  In order to respond accurately and reliably to these issues, FILAB offers tailor-made support for particle identification in your DMs according to AAMI TIR42 but also USP788, PE 2.9.19, and ISO 19227...Particle extraction and counting on implants - AAMI TIR42 methodologyParticle counting on implantable DM by Optical MicroscopeParticle contamination analysis Identification of particles in your pharmaceutical solutions by Scanning Electron Microscopy (SEM)Analysis of your pharmaceutical solutions by infrared microscopy (FTIR)Analysis and identification of particles in your pharmaceutical solutions by ICP-MS, ICP-AESFor more information, consult our expert's word or contact us : contact@filab.fr - tel : 03.80.52.32.05 or ask for a quote here. Request a quote What are the analysis methodologies preconised by AAMI TIR42? AAMI TIR42 is a guidance document that provides recommendations on how to test medical device materials for chemicals that may pose a risk to patient safety. To identify and quantify these chemicals, AAMI TIR42 recommends using several different analysis methods. One of the recommended analysis methods is gas chromatography-mass spectrometry (GC-MS), which is used to separate and identify small molecules in complex mixtures. This technique involves looking at the individual components of a mixture and analyzing their physical properties to determine what they are. Another method is high-performance liquid chromatography (HPLC), which is used to separate and identify organic molecules in complex mixtures. This technique is particularly useful for identifying chemicals that may be present in very small amounts. A third recommended analysis method is Fourier transform infrared spectroscopy (FTIR), which is used to identify the chemical functional groups present in a material. FTIR works by analyzing the wavelengths of light that are absorbed by a sample, which can reveal the different chemical bonds present. X-ray photoelectron spectroscopy (XPS) is another recommended analysis method. This technique is used to identify and quantify the elements present in a sample. It works by irradiating the sample with X-rays and measuring the energy of the electrons that are emitted. Finally, inductively coupled plasma optical emission spectroscopy (ICP-OES) is recommended for determining the elemental composition of a sample. This technique involves ionizing the sample and measuring the wavelengths of light emitted by the excited atoms. AAMI TIR42 recommends several different analysis methods for identifying and quantifying chemicals in medical device materials, including GC-MS, HPLC, FTIR, XPS, and ICP-OES. These techniques help to ensure that medical devices are safe for patient use by identifying any potentially harmful chemicals that may be present Why is it important to perform particle contamination counting according to AAMI TIR42 standards? Particle contamination counting is an important aspect of testing for medical device materials, as it can help to ensure their safety and effectiveness. AAMI TIR42 provides guidelines on how to perform particle contamination counting to detect any microscopic particles that may be present in the material. Particles can come from various sources, including the manufacturing process, the environment, or the materials themselves. They can be foreign bodies in the material, or they can be generated by the wear and tear of the device as it is used. Particle contamination can lead to a host of problems, including inflammation, thrombosis, and other adverse reactions, making it important to detect and measure the degree of contamination. AAMI TIR42 recommends performing particle contamination counting using optical microscopy, which involves examining a sample of the material under a microscope to count and categorize the particles present. The size, shape, and composition of the particles can also be assessed to determine their potential impact on the device's safety and effectiveness. By performing particle contamination counting according to AAMI TIR42 standards, medical device manufacturers can identify and quantify any particle contamination present in their materials and take appropriate action to ensure the safety and efficacy of their devices. This is especially important for medical devices that will be implanted or used in close contact with the body, as particle contamination can have serious consequences for patient health.  Why should you externalize your particle contamination counting? Externalizing your particle contamination counting can be beneficial for several reasons, particularly in ensuring that you are obtaining accurate and unbiased results. AAMI TIR42 recommends that particle contamination counting should be performed by an external testing laboratory that specializes in this type of analysis.Externalizing particle contamination counting allows for an objective evaluation of the materials. An external laboratory has no vested interest in the outcome of the analysis, which can help to ensure that the results are impartial and accurate. Additionally, external laboratories may have access to specialized equipment or techniques that are not available in-house, providing a more comprehensive and detailed analysis.It ensures compliance with regulatory requirements. External laboratories are often accredited by regulatory bodies and must adhere to strict quality control measures, ensuring that their analysis meet the highest standards. By outsourcing particle contamination counting to an accredited laboratory, medical device manufacturers can demonstrate to regulatory agencies that they are following best practices and complying with relevant standards, such as AAMI TIR42.Finally, externalizing particle contamination counting can save time and resources. Performing this type of analysis in-house requires investing in specialized equipment, training personnel, and dedicating valuable lab space. By outsourcing to an external laboratory, medical device manufacturers can free up resources to focus on other areas of product development and ensure timely and accurate results.
Sectors of activity Measurement of Zeta potential on cosmetic products Your needs: analyse the Zeta potential of your finished products and raw materials What is Zeta potential? Zeta potential, also known as electrokinetic potential, is a measure of the electrical charge that forms on the surface of suspended particles when they are dispersed in a liquid. This charge influences the way the particles interact with each other, affecting their stability.Zeta potential analysis can therefore be used to assess the stability of cosmetics such as suspensions, emulsions and nanoparticles by measuring the surface charge of the particles. Measuring zeta potential The measurement of zeta potential is used to determine the colloidal stability of formulations by assessing the surface charge of particles. A high zeta potential promotes stability by keeping particles dispersed, thereby reducing the risk of aggregation.In addition, zeta potential analysis offers valuable insights into the causes of dispersion, aggregation or flocculation, helping to improve the formulation of dispersions, emulsions or suspensions, ensuring more effective and longer-lasting products.As a result, zeta potential measurement has important applications in a wide variety of industries, including cosmetics, pharmaceuticals, chemicals, electronics, water treatment, etc. Analysis of zeta potential in cosmetics and pharmaceuticals In the cosmetics industry, zeta potential is measured to assess the stability of emulsions and suspensions. Creams and lotions, which are often emulsions, need to maintain a homogenous dispersion of particles to ensure their effectiveness and shelf life. By measuring the zeta potential, it is possible to assess the stability of these products, helping to avoid phase separation, a common problem in cosmetic formulations.In pharmaceuticals, galenic formulations, such as suspensions and injectable solutions, require zeta potential analysis to ensure the stability of active particles, avoiding aggregation that could compromise therapeutic efficacy.The aim of zeta potential measurement is toimprove the long-term stability of the solution by modifying the pH, additive concentration or ionic strength. Why carry out a zeta potential analysis? Zeta potential analysis is used in a variety of situations where an understanding of particle stability and surface interactions is required. Here are a few cases where zeta potential analysis is particularly relevant: Improved suspension stability: in products such as paints, inks, cosmetics and pharmaceuticals, where preventing particle aggregation is crucial to product quality. Product formulation: to develop stable emulsions, creams, lotions and other formulations where particle size and charge can affect the properties of the final product. Nanotechnology research and development: In the design of nanoparticles for medical, electronic or catalysis applications, where the surface charge can influence the interaction with cells, substrates or other particles. Materials science: In the analysis of the surface of porous materials, ceramics, polymers, etc., where surface properties influence product performance. Biotechnologies and medical sciences: to study the stability of proteins, vaccines, viruses and other biological systems. Quality control: to ensure that the properties of the particles remain within the desired specifications during production and storage. The FILAB laboratory assists manufacturers with their problems by offering to measure Zeta potential. With state-of-the-art analytical equipment and a qualified team of doctors and engineers, the FILAB laboratory analyses and measures the zeta potential of your finished products or raw materials.The measurement and control of zeta potential is essential in product research and development, enabling the creation of safe, effective and pleasant products. our zeta potential measurement services Measurement of zeta potential on a cream Measurement of Zeta potential on inorganic pigments Measurement of zeta potential on a powder Measurement of Zeta potential on a suspension Measurement of zeta potential in a nanoparticle solution Our technical resources Measurement of zeta potential is based on advanced techniques, mainly electrophoretic mobility and dynamic light scattering (DLS). Electrophoretic mobility measures the speed at which particles move under the influence of an electric field, providing the value of the zeta potential. The analysis of surface charge is a related subject, as the zeta potential is a manifestation of this charge at the interfaces between the particles and the surrounding liquid.Our state-of-the-art equipment enables us to obtain accurate and reproducible results, which are essential for assessing the colloidal stability of formulations. Zeta potential for suspensions and nanoparticles Zeta potential is a key indicator for the stability of suspensions and nanoparticles in cosmetics and pharmaceuticals. A high zeta potential value indicates that particles in suspension have a strong electrostatic repulsion, reducing the risk of aggregation. This is particularly important for products containing nanoparticles, where uniform dispersion is essential for product efficacy. Importance of zeta potential in galenics Zeta potential is used to check the stability of suspensions and emulsions. It assesses the surface charge of particles, influencing their ability to remain dispersed. Adequate zeta potential prevents aggregation and sedimentation, ensuring controlled release of active ingredients and improved therapeutic efficacy. By incorporating this measure, galenic formulations can be optimised for maximum performance. OUR additional analyses Organic chemical analysis: GCMS, Py-GCMS, LC-MSMS, GPC, NMR, FTIR Inorganic chemical analysis: ICP, DRX, CI Thermal analysis: ATG, DSC Particle size distribution by DLS Metallurgical analyses: ICP, MEB-FEG EDX, SEO Powder analysis: XRD, SEM-FEG EDX, BET. Surface analysis: SEM-FEG EDX, XPS, TOF-SIMS FAQ Why should I carry out a zeta potential analysis on my products or raw materials Zeta potential analysis is essential for assessing the stability of suspensions, emulsions and nanoparticles in your products. It helps prevent problems such as particle aggregation or phase separation. What types of products can benefit from a zeta potential analysis Cosmetics, pharmaceuticals, foodstuffs and high-tech materials such as nanoparticles can all benefit from this analysis. It is particularly useful for emulsions, suspensions and other formulations requiring stable particle dispersion. How does zeta potential influence the stability of suspensions and emulsions? A high zeta potential indicates a strong repulsion between particles, reducing the risk of aggregation and improving the stability of the suspension or emulsion. Conversely, a low zeta potential can lead to particle coalescence, compromising product quality. What causes flocculation in an emulsion or suspension Flocculation occurs when the zeta potential is insufficient to keep suspended particles separated, leading to the formation of flocs or clusters, thus affecting the stability of the product. How can I assess the colloidal stability of my formulations? Colloidal stability can be assessed by measuring the zeta potential, which indicates the force of repulsion between particles in suspension. A high zeta potential suggests good stability, reducing the risk of aggregation or flocculation. What are the signs of insufficient colloidal stability in my formulations Signs of colloidal instability include particle aggregation, sediment formation or phase separation, indicating that the zeta potential is too low to maintain a uniform dispersion.
Our services Training in surface analysis objectives In-depth understanding of the mechanisms governing surface properties Ability to interpret the results of analyses to guide decision-making on product development or process improvementsn de processus Ability to select and apply appropriate surface analysis techniques according to the specific needs of a project or research project Pedagogical resources Screening of training materialHandover of training materialTraining led by experts in the techniques required Target audience Technicians or engineers in charge of research & innovation, process & industrialisation, production & maintenance, quality control, health, safety & environment, purchasing & supplies ... Program For more information on the program, please contact us Information updated on 07.10.2024 Practical information In-company trainingQuestionnaire at the beginning and end of the course (Quizzes)Attendance sheetDuration: 2 daysPRM and PSH accessibilityAdaptable to customer needsPrice on quotationNo pre-requisites required for this courseA certificate of completion will be issued at the end of the course. PRM and PSH access Our training courses are accessible to people with disabilities. We will offer you solutions for adaptations (e.g. training aids, pace of training, teaching support, etc.) and adjustments to suit your needs. Your teams need training in suface analysis What is the principle of surface analysis techniques?The term surface analysis refers to the surface of a material. This is a vulnerable area where many interactions exist with its environment. This zone is endowed with several so-called specific characteristics, so that the material responds to the performances afterwards. The knowledge of the properties and surface states of a material can allow you to adapt your manufacturing processes. Thus, it is possible to implement surface treatment or cleaning processes.Why train in surface analysis?Understanding the properties and conditions of a material's surface is crucial. It enables you to adjust your production methods accordingly, by incorporating specific surface treatment or cleaning techniques.The applications of surface analysis are many... you will be able to..: solutions Analyze the chemical composition of the surface of a material Characterize the surface coating Validate cleaning processes Analyze and characterize surface treatments Characterize the surface treatment baths Study the morphology of the surface of a material (porosity, roughness,...) Study failures and surface defects (cracking, rupture, migration, corrosion...) Développer les traitements de surface Identify surface pollution (analysis of particles, deposits, etc.) Conducting aging studies FILAB's surface analysis training... When should a surface analysis be carried out? You wish to answer your problems of surface analysis? You have just acquired different technical means to perform a surface analysis (SEM-FEG EDX, Optical Microscope, BET, µ-IRTF) in your laboratory? The competent person(s) are no longer part of your team? You wish to improve your expertise on surface analysis and the exploitation of the results? Why choose FILAB for your surface analysis training courses? As an accredited training organization, FILAB supports your teams in the use of surface analysis techniques, regardless of your sector of activity.At FILAB, we develop and offer our customers tailor-made training courses that are in line with your industrial issues or analytical challenges.  Technical resources used in surface analysis training MEB-EDX Microscope Optique AFM TOF-SIMS XPS AFM To register for the course or to obtain a quote, please contact us directly by email or telephone.Training will start within 3 months of acceptance of the agreement.
Our services Characterization of the rouging in laboratory You want to characterize rouging on your materials? What is rouging? Rouging is a very thin film that appears as a result of a disturbance of the outer layer of the surface of stainless steels. The formation of iron oxides and other metal oxides is thus favored and leads to the coloration of the surface.  Rouging is characterized in particular by a coloration of the surfaces of certain stainless steel equipment, from yellow to black, through orange and red, depending on the extent of the phenomenon. Why characterize the rouging on your materials? Rouging is not a spontaneous phenomenon. In fact, the appearance of rouging is characteristic of a failure generally linked to the surface treatment. It also implies that the steel loses its anti-corrosion properties and its resistance. Thus, the characterization of rouging by a specialized laboratory is essential in the optimization of your materials. FILAB supports you in the characterization of rouging on your materials Through our three levels of services: analysis, expertise and R&D support, FILAB assists companies of all sectors and sizes.  Indeed, FILAB supports you in the characterization of rouging and takes charge of the different steps of realization. Thanks to its high level of in-house expertise and diversified analytical resources, FILAB can offer you solutions tailored to your needs. Thus, our laboratory provides you with several analytical techniques: Time-of-flight Secondary Ion Mass Spectrometry (TOF-SIMS). This method allows, to begin with, to obtain elementary and molecular information on the species present on the extreme surface of samples X-ray photoelectron spectroscopy (XPS/ESCA). This method allows then to determine the elemental chemical composition of a material on a depth of a few nanometers. Scanning Electron Microscopy (SEM/EDX). Finally, this method allows morphological observations and local semi-quantitative chemical analysis on the product go further Laboratory audit and team training Support in the optimization of production processes Expertise in analytical chemistry Study of failures: study of fracture surfaces, analysis of contamination or particles, adhesion problems, corrosion phenomena, metallographic examination, weld analysis...  Deformation Request a quote The positive aspects of FILAB A highly qualified team Responsiveness in responding to and processing requests A complete analytical park of 5 200m² Tailor-made support
Our services Analysis of rouging phenomenon in laboratory Your needs: analyze the rouging phenomena on your products What is rouging? Rouging is a phenomenon that occurs when the outer layer of the surface of stainless steels is disturbed. The formation of iron oxides and other metallic oxides (nickel or chromium) is thus favored and leads to the coloration of the surface.  A very thin film, rouging is characterized by a coloration of the surfaces of certain stainless steel equipment, from yellow to black, through orange and red, depending on the extent of the phenomenon. Why analyze the rouging phenomenon on your products? Rouging does not occur spontaneously. In other words, rouging is a symptom of surface degradation of stainless steel. It also implies that the steel is losing its corrosion resistant properties and strength. Furthermore, rouging is unstable and not an acceptable phenomenon in many processes. Indeed, the oxidation particles can detach and contaminate the possible transported products, which endangers the safety of the processes. Request a quote FILAB supports you in the analysis of rouging phenomena Through our three levels of services: analysis, expertise and R&D support, FILAB assists companies of all sectors and sizes.  Indeed, FILAB accompanies you in the analysis of rouging phenomena and takes charge of the different stages of realization. Thanks to its high level of in-house expertise and diversified analytical equipment, FILAB can offer you solutions tailored to your needs. Thus, our laboratory provides you with several analytical techniques: Time-of-flight Secondary Ion Mass Spectrometry (TOF-SIMS). This method allows, to begin with, to obtain elementary and molecular information on the species present on the extreme surface of samples X-ray photoelectron spectroscopy (XPS/ESCA). This method allows then to determine the elemental chemical composition of a material on a depth of a few nanometers. Scanning Electron Microscopy (SEM/EDX). Finally, this method allows morphological observations and local semi-quantitative chemical analysis on the product go further Laboratory audit and team training Support in the optimization of production processes Expertise in analytical chemistry Study of failures: study of fracture surfaces, analysis of contamination or particles, adhesion problems, corrosion phenomena, metallographic examination, weld analysis...  Deformation Request a quote The positive aspects of FILAB A highly qualified team Responsiveness in responding to and processing requests A complete analytical park of 5 200m² Tailor-made support
Our services Validation of surface treatment processes You wish to validate the performance of your surface treatment processes... First of all, it is important to understand why you need to validate your surface treatment processes. Indeed, whether you are in a context of development of a component, a product ... etc., you want on the one hand, to protect it or on the other hand, optimize it. Surface treatment to protect The development of a product includes many phases, among them, the ability to perform.  Thus, to meet this last phase, the protection by surface treatment of your product is essential.Surface treatment to optimizeYou are facing several problems of failures on your surface treatment... Thus, to understand why this treatment fails, it is advisable to carry out an analysis of surface treatment.If you already know the cause of the problem and wish to improve the surface treatment, FILAB can help you validate new surface treatment processes on your products.Finally, the validation of surface treatment processes allows you to continue to develop your product and adapt your manufacturing process with complete peace of mind.  The technical means of the FILAB laboratory to validate your surface treatments FILAB supports you in the validation of all types of surface treatment processes such as  by chemical treatment by shot blasting by passivation by anodizing Our means of analysis and characterization of surface treatments are also multiple, depending on the nature of the treatment: Scanning Electron Microscope (SEM-FEG EDX): chemical and morphological analysis, thickness control, homogeneity Analysis by AFM TOF-SIMS analysis, XPS for extreme surface examination  FTIR analysis Request a quote Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Thickness measurement by SEM in laboratory You want to measure the thickness of the surface treatment by SEM? To begin with, scanning electron microscopy is an electron microscopy technique. This method allows the analysis of a material by a fine beam of electrons that scans the surface of the material without destruction. Thus, at the end of this analysis, several information can be obtained in particular, the thickness of the various layers.The measurement of the thickness of the different layers of a material by SEM, allows you, first of all, to check and adapt your manufacturing processes. Indeed, the SEM, by the quality of the image obtained at the end of the analysis, makes possible the meticulous observation of the various layers.In addition, electron microscopy also allows you to adapt the implementation of surface treatment or cleaning processes. FILAB assists you in the measurement of thickness by SEM on all types of materials Through our three levels of services: analysis, expertise and R&D support, FILAB assists companies of all sectors in the analysis of material contamination by SEM. For this purpose, FILAB provides its customers with the know-how and experience of its team as well as a 5 200m² analytical park with state-of-the-art equipment.In addition, FILAB has significant experience in the measurement of layer thickness by SEM and the development of specific methods.  Example of services Analysis of the chemical composition of the surface by SEM-FEG-EDX, XPS or TOF-SIMS Morphological study of the surface of a material (porosity, roughness,...) by SEM-FEG-EDX Characterization of the surface coating by SEM-FEG-EDX Analysis and characterization of surface treatment by SEM-FEG-EDX Identification of surface pollution (analysis of particles, deposits,...) by SEM-FEG-EDX Study of failures and surface defects by SEM-FEG-EDX (crack, rupture, migration, corrosion...) Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Study of delamination phenomena in the laboratory What is delamination? In industry, delamination is the property of a material to shear through its thickness longitudinally.The phenomenon of delamination concerns complex films and laminated composite materials. It can also occur on fibers, on steel parts with a protective layer, in materials composed of polymers.The support and guidance of an analysis laboratory with specific techniques for the study of surface coatings allow manufacturers to gain in efficiency and quality on their materials.  Study of delamination phenomena: a specific expertise of the FILAB laboratory For more than 30 years, the FILAB laboratory has had the experience and specific analytical equipment to meet the need for expertise on materials, and in part the study of delamination phenomena on all types of materials (metallic, polymer, films...). The following techniques can be solicited: Microstructural observation by Optical Microscope and Scanning Electron MicroscopeExtreme surface analysis by TOF-SIMS and XPSIdentification of surface pollution (analysis of particles, deposits,...)Study of failures and thickness defects by SEM (crack, rupture, migration, corrosion...)Development of surface treatment processesRoughness analysis by AFMThrough our three levels of services - analysis, expertise and R&D support - FILAB assists companies of all sectors and sizes in solving their industrial problems, by providing its clients with the know-how and experience of its team. For more information, contact our expert at contact@filab.fr - tel: 03.80.52.32.05 Contact us Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Multi-layer analysis of material surfaces in the laboratory You want to perform multi-layer analysis on the surface of your materials? Surface and multilayer analysis in a few words... What is called a surface is a vulnerable zone where the interactions between the material and its environment take place. This area is endowed with several so-called specific characteristics, so that the material responds to the performance afterwards. As for the multi-layer surface analysis, it is an analysis performed on several surface layers of a material. It is a method of analysis widely used to determine the composition of the surface of a material.Indeed, the multi-layer analysis of the surface of a material makes it possible to determine the number of layers, the composition of each as well as to measure the thickness of each one. Why perform a multi-layer analysis on the surface of your materials? The multi-layer analysis on your materials allows you, first of all, to determine with precision the composition of the surface of your materials. Moreover, it is an essential analysis when studying the failure of your materials. Indeed, several failures can be observed such as corrosion, coating failure, adhesion problems...Thus, the knowledge of the properties and surface states of a material can allow you to adapt your manufacturing processes. Thus, it is possible to implement specific processes to your needs. FILAB supports you in the multi-layer analysis of the surface of your materials Through our three levels of services: analysis, expertise and R&D support, FILAB assists companies of all sectors in the multi-layer analysis of the surface of materials. FILAB provides its customers with the know-how and experience of its team as well as a 5 200m² analytical park with state-of-the-art equipment.In addition, FILAB has significant experience in the implementation of multilayer analysis of material surfaces and the development of specific methods.  Our technical means Scanning Electron Microscopy SEM-EDX  Time-of-flight Secondary Ion Mass Spectrometry (ToF-SIMS) X-ray photoelectron spectroscopy (XPS) Atomic Force Microscope (AFM) examples of services Study the morphology of the surface of a material (porosity, roughness,...) Study failures and surface defects (cracks, breaks, migration, corrosion...) Conducting aging studies Develop surface treatments Identify surface pollution (analysis of particles, deposits, etc.) Characterize the surface treatment baths Request a quote Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Surface analysis by X-ray tomography How to check the conformity and surface performance of your material by X-ray tomography? First of all, surface analysis allows to define the properties and surface state of a material.  X-ray tomography is a means to answer this definition. Indeed, its purpose is to check the conformity and the performance of your material.How does X-ray tomography do this? By studying...the composition of the material,the surface at its heart,and following its evolution according to external constraints.This is a technique of analysis and control of materials by imaging using the interaction of radiation and matter. It allows to build 3D images of the studied surface. In addition, it is a very popular technique in some industrial sectors because it is not necessary to destroy the material to analyze it. Thus, to control the conformity and the performance of your material, it is advisable to carry out a surface analysis by X-ray tomography.  FILAB supports you in your surface analysis needs by X-ray tomography With significant experience in surface analysis and material characterization, FILAB Laboratory can help you understand the behavior of your products and find appropriate solutions.FILAB Laboratory uses, among others, X-ray tomography analysis, but also state-of-the-art tools such as FEG-EDX SEM, XPS or AFM.  to go further Surface analysis by SEM Morphological characterization of materials BET Analysis and Specific Surface Area Measurement (SSAV) Extreme surface analysis by TOF-SIMS and XPS Request a quote Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Surface roughness analysis What is surface roughness? The surface of a material is a vulnerable zone where many interactions with its environment take place. It conditions, by its specific characteristics, the global performances of materials. It can impact the reliability and the solidity of a product in case of failures (corrosion, wear, adhesion, friction...).Moreover, whatever its manufacturing process, the surface is not perfectly smooth. Indeed, this can depend on various factors such as: the machining method, the tools used, the materials. These materials have many irregularities that can be called defects.  All these surface defects constitute the roughness.Shape : Deviations over long periods or non-cyclic deviationsRipples: Surface structure with longer intervals of irregularities.Roughness : Irregularities with short intervals Why is surface roughness important? Each production process has an impact on the quality of the surface and thus leads to the appearance of roughness. In this context, the FILAB Laboratory supports you in your surface roughness issues through the following services:  Roughness analysis by AFM, SEM-EDX, XPS Surface treatment analysis Morphological study of the surface Failure study Request a quote Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
Our services Analysis of the surface topography What is topography? Topography is part of a surface analysis context.Many interactions remain on a material surface. These play a major role in the behavior of the material, in order to better understand them, surface analysis is necessary.Finally, the surface topography manifests itself on three levels: Macrographic, the surface is the limit between the solid and its environmentMicroscopic, the surface presents numerous irregularities and mechanical alterations. These are superimposed on the shape defects. The "microscopic" level aims at the geometry of the roughness profileNanometrically, the surface can be schematized by an irregular stacking of atoms with a discontinuity in the arrangement of the atoms of the solid which confers to the surface atoms an intrinsic energy higher than those of the volume. Moreover, the properties and surface states of a material allow an adaptation of the manufacturing processes. What parameters are obtained from the surface topography? Topographic surface analysis is used for various applications such as: Analysis of the surface condition of a materialAnalysis of roughnessThe study of a surface defectPhase identificationStructural analysis of a surfaceEtc. FILAB supports you in your topographic analysis needs... The FILAB laboratory is equipped with an analytical park of more than 2000m² to meet your needs for chemical and physical analysis of surfaces and topographic examinations:  Atomic Force Microscopy (AFM) Optical Microscope (OM) TOF-SIMS MEB-EDX XPS Request a quote Les + FILAB Une équipe hautement qualifiée Une réactivité de réponse et de traitement des demandes Un laboratoire accrédité COFRAC ISO 17025 (Portées disponibles sur www.cofrac.com - N° accréditation : 1-1793) Un parc analytique complet de 5 200m² Un accompagnement sur-mesure
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