Heavy metals analysis in the laboratory

Chemical analysis R&D support
More than 120 people
More than 120 people at your service
5200 m² laboratory
5200 m² laboratory + 99% of services are provided in-house
Accredited laboratory
Accredited laboratory COFRAC ISO 17025

Your needs : to ensure that your products are comply with regulations regarding heavy metals

Indispensable in industry, heavy metals are subject to in-depth analysis and strict regulations. Industrial companies must integrate the control and analysis of heavy metal content and presence in their finished products and raw materials. As a result, their use is highly regulated in industrial sectors such as cosmetics and pharmaceuticals.

What is a heavy metals analysis?

Heavy metal analysis is a laboratory technique used to determine the quantity of metals present in a sample. This analysis is of vital importance in many industrial sectors. Heavy metal analysis can detect the levels of these substances in a given sample, enabling compliance with regulations.

Heavy metals to control in your materials and substances

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Heavy metals analysis

Heavy metals are chemical elements with a density greater than 5 g/cm3. These metals are environmental pollutants that can be released into the air, water and soil by various industrial and anthropogenic activities. The list of metals considered as heavy metals includes :

Why use a heavy metals analysis laboratory?

Heavy metals analysis is one step in determining the quality of a sample. Heavy metals are naturally occurring elements, but their excessive accumulation in water, soil or air can be dangerous.

Indeed, heavy metals such as lead, mercury and cadmium can be toxic to human and animal health, as well as to the environment. Some heavy metals can accumulate in living organisms and affect their functioning, with negative effects on human health and biodiversity. This is why their use and release into the environment are regulated.

Our solutions: control and analyze the presence of heavy metals with competitive prices and lead times

Our technical resources dedicated to the analysis and determination of heavy metals

The FILAB laboratory puts its expertise and state-of-the-art analytical equipment at your disposal for metal analysis, and in particular the analysis of heavy metals (lead, mercury, arsenic, cadmium, nickel, antimony, etc.) on any type of material.

Analytical techniques such as ICP-MS (inductively coupled plasma mass spectrometry) are used to accurately measure the concentration and distribution of these metals in a sample, which can enable rapid, targeted intervention. In addition, heavy metal analysis can also help identify sources of contamination that may be linked to industrial, agricultural or other activities.

Services adapted to each sector:

Screening and determination of heavy metals using ICP-MS or ICP-AES in chemical matrices : treatment baths, materials, raw materials…

Quantitative analysis of heavy metals in cosmetic products using ICP-MS : lipstick, mascara, eyeliner…

Inorganic analysis

Determination of heavy metals or trace amounts of catalysts in packaging materials

Mercury analysis using an amalgamator

ICP-MS heavy metal analysis of raw materials used in cosmetics : natural mica, sericites, metallic oxides (Titanium oxide, Zinc oxide, Iron oxides…), talc, clay…

Elemental impurity analysis of pharmaceutical products using ICP in accordance with USP 233 (ICH Q3D standard)

Determination and analysis of Chromium VI

Metallic impurity analysis of Medical Devices and of cosmetic products

Analytical development and validation using ICP-MS or ICP-AES  

Metal analysis regulations

Analysis of the presence of heavy metals in industry is a major concern in Europe. Companies are subject to strict legal obligations to analyze their pollutant emissions and the impact of their activities on the environment. In this context, heavy metal analyses are a priority for the competent authorities. Companies must therefore ensure that their emissions comply with European environmental safety and public health standards, by having a metals analysis carried out by a competent laboratory.

métaux lourds

Regulatory requirements for heavy metals

To find out more about the legal requirements for heavy metal analysis in industry, please refer to the following regulations:

General Regulation (EC) N°1881/2006 of the European Union

European Union General Regulation (EC) No. 1881/2006: This regulation sets regulatory values for heavy metals in foodstuffs, including lead, cadmium and mercury.

Directive n° 86/278/CEE

This directive concerns the protection of the environment, and in particular soil, when sewage sludge is used in agriculture. It establishes detection limits for each metal to guarantee soil quality.

European Reach Directive

The European Reach Directive (Registration, Evaluation, Authorization and Restriction of Chemicals) aims to improve protection of human health and the environment by regulating the manufacture, import and use of chemical substances, including heavy metals.

RoHS Directive

The RoHS (Restriction of Hazardous Substances) Directive restricts the use of certain hazardous substances, including heavy metals such as lead, mercury, cadmium and hexavalent chromium, in electrical and electronic equipment sold on the European market.

As legal requirements can vary from one country to another in Europe, it is essential to refer to the specific regulations of each country to find out the exact legal obligations concerning the analysis of heavy metals in industry. Do you need help? Filab can help you understand your needs and advise you on the metal analyses required for your business.

FILAB ISO 17025 accreditations

COFRAC ISO 17025 accreditation is a form of recognition for analytical laboratories. It attests to the competence of laboratories to carry out precise tests and calibrations to quantify the presence and concentration of substances, particularly heavy metals, in samples. FILAB’s COFRAC ISO 17025 accreditation is a guarantee of confidence for industry.

Since October 2015 FILAB laboratory has been ISO 17025 accredited by COFRAC for the determination of metallic impurities in raw materials and in pharmaceutical products, in accordance with standards described in the European Pharmacopoeia 2.4.20 and the American Pharmacopoeia USP 233.

FAQ

How are heavy metals measured?

Analysis laboratories can use a variety of techniques to measure heavy metals in a product.

The most commonly used technique is atomic absorption spectrometry (AAS). This method involves vaporising the product to be analysed to create a cloud of atoms that are then excited by a light source. The heavy metals present in the cloud will absorb some of this light, enabling their concentration to be measured.

Another method often used is X-ray fluorescence spectrometry (XFS). This technique uses a source of X-rays to excite the heavy metals present in the product. The metals then emit a fluorescence that can be used to measure their concentration.

There are also other methods such as ion chromatography, mass spectrometry and voltametry, which can be used depending on the type of product to be analysed and the sensitivity required for heavy metal detection.

In all cases, it is important to follow strict protocols to ensure accurate and reliable results. Analysis laboratories must comply with strict quality standards and use state-of-the-art equipment to carry out these important analysis.

How can companies prevent heavy metal contamination in their manufacturing processes?

There are a number of measures that companies can take to prevent heavy metal contamination in their manufacturing processes. Here are a few examples:


Identify potential sources of contamination: Companies should carry out a thorough assessment of their manufacturing processes to identify potential sources of heavy metal contamination. This may include the use of raw materials containing heavy metals, inadequate processing or handling equipment, or discharges of contaminated industrial wastewater.


Implement quality control procedures: Companies should implement quality control procedures to ensure that finished products do not contain excessive amounts of heavy metals. This may include the use of regular heavy metal assays and compliance verification protocols, as well as the establishment of strict production standards.


Use safer substitutes: In some cases, companies may be able to use safer substitutes to replace heavy metals in their manufacturing processes. More environmentally friendly and sustainable alternatives can be used to replace products containing heavy metals.


Educate employees: Companies need to educate and train their employees on the risks associated with heavy metal contamination and the preventive measures that need to be put in place to minimise the risks. Employees must be informed about safety procedures, personal protective equipment and emergency protocols.

When should an arsenic assay be carried out?

Reminder: what is arsenic?
Arsenic is a chemical element with an electronic configuration similar to that of phosphorus, and is located just above it on the periodic table. Like phosphorus, arsenic can form covalent bonds with other elements. However, it also has metallic properties, making it useful for making alloys. Arsenic is used in many fields, including the semiconductor industry, alloy manufacture, agriculture (in the form of pesticides) and medicine (in certain cancer treatments). However, excessive exposure to arsenic can be harmful to health, as it is toxic to human cells. Arsenic is also considered a known human carcinogen.

Arsenic is frequently dosed in industry for several reasons. Firstly, arsenic can be a common contaminant in various types of industrial chemicals and processing agents. Companies that produce or use these chemicals may be required to carry out regular tests to check for the presence of arsenic in their samples.

In addition, arsenic may be present in soil samples as a result of environmental contamination. Analysis laboratories may therefore be asked to carry out tests on soil samples taken from industrial areas or which have been exposed to chemicals containing arsenic.

Finally, laboratories can carry out arsenic measurements as part of scientific research studies. Scientists can study the effects of arsenic on the environment, pharmacology and other related subjects. An arsenic assay is needed to measure the concentration of arsenic in samples and to understand how it interacts with other chemical compounds.

When should a phthalates assay be carried out?

Phthalates can be dosed in a variety of different ways. Phthalates are chemical compounds commonly used as plasticisers to improve the flexibility, durability and performance of many plastic products. However, they can also be toxic to human health at high concentrations.

Here are some examples of why phthalates may need to be dosed:

In the children's toy industry: Phthalates can be present in children's plastic toys. In many countries, there are strict regulatory standards concerning the amount of phthalates permitted in children's toys. Phthalate dosages are essential to ensure that toys do not contain dangerous quantities of these chemical compounds.

In the food industry: Studies have shown that phthalates can migrate from plastic food packaging into the food it contains. Phthalate testing is therefore necessary to ensure that foods do not contain harmful levels of these chemicals.

In the textile industry: Phthalates can also be found in soft plastic or vinyl clothing, as well as in certain types of synthetic leather. Phthalate dosages are essential to ensure that garments do not contain dangerous quantities of these chemical compounds.

In the medical industry: Phthalates can be used in plastic medical devices such as catheters and blood bags. Phthalate testing can help to ensure that devices do not contain harmful levels of these chemicals.

The filab advantages
A highly qualified team
A highly qualified team
Responsiveness in responding to and processing requests
Responsiveness in responding to and processing requests
A COFRAC ISO 17025 accredited laboratory
A COFRAC ISO 17025 accredited laboratory
(Staves available on www.cofrac.com - Accreditation number: 1-1793)
A complete analytical park of 5,200m²
A complete analytical park of 5,200m²
Tailor-made support
Tailor-made support
Clément BOENARD Head of Inorganic Chemistry Department
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