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Analysis of steels according to ASTM E3515 by ICP-AES

Addressing the challenges of steel chemical composition

Control of chemical composition determines the mechanical properties, weldability, corrosion resistance and fitness for use of steel. In production, during a failure investigation or as part of supplier quality control, a variation in elemental content can compromise the compliance of a grade or the interpretation of a quality deviation.

An analysis of steels performed according to a suitable protocol makes it possible to quantify the constituent and residual elements present in the material. The Filab laboratory assesses your requirements with regard to the ASTM E3515 analysis reference, the metallic matrix, the elements being investigated and the applicable decision thresholds.

Defining the elements to be measured according to the grade and application

ICP-AES is suitable for the simultaneous investigation of numerous metallic elements present in steels. Depending on the requirements, the analytical program may target chromium, nickel, molybdenum, manganese, copper, silicon, vanadium, titanium, niobium, cobalt or aluminum, among others.

The final list of elements is defined with the client based on the target grade, specifications, material requirements or investigation objectives.

Analyzing parts, chips, powders and metallic products

The Filab laboratory can examine metal parts, coupons, chips, powders, wires, sheets, bars or fragments taken from an identified area. The sample should be accompanied by useful information: material designation, product history, sampling area, elements to be investigated and compliance requirements.

Obtaining multi-element measurements after dissolution

The ICP-AES analysis makes it possible to measure several elements in the same test solution. It is a relevant solution for characterizing the elemental composition of steel, comparing a material with a specification or investigating a composition nonconformity.

Steel analysis by ICP-AES at the Filab laboratory

The Filab laboratory uses ICP-AES analysis for multi-element determination in steels, following preparation and dissolution adapted to the nature of the sample. This approach supports industrial companies in the inspection of raw materials, finished parts, semi-finished products, rejects or metallic deposits.

Each request undergoes a technical review to define the elements to be measured, the required sample quantities and the expected reporting format. For additional requirements related to metallurgical processes, discover how Filab supports foundry industry professionals.

Adapting sample preparation to the steel matrix

The quality of the result depends on the representativeness of the sample and its preparation. Before dissolution, the Filab laboratory examines the surface condition, geometry, any coatings and potential heterogeneity. This step makes it possible to adapt the protocol to the matrix and ensure reliable interpretation of the measured concentrations.

Ensuring sample representativeness

When composition may vary between different areas, a targeted sampling plan can distinguish the bulk material, a heat-affected zone, a weld or a deposit. The Filab laboratory can guide sample preparation so that the analysis of steels addresses the industrial question at hand.

Matching the method to the inspection objective

The choice of method depends on the target elements, expected concentrations, nature of the matrix and acceptance criteria. The Filab laboratory verifies the suitability between the objective of the ASTM E3515 analysis and the required analytical performance. For other standards-related requirements, consult our analysis laboratory according to ASTM E165.

Submit your analysis request and requirements

To prepare your project, provide the reference of the applicable standard or specification, the steel designation, the elements to be tested, the number of samples, and your target turnaround time. The Filab laboratory will assess the analytical feasibility and define a suitable proposal.

Contact the Filab laboratory, send your samples, and obtain a quote for your steel analysis by ICP-AES.

Frequently asked questions

How can the chemical composition of steel be controlled according to ASTM E3515 using ICP-AES?

ICP-AES analysis is based on the controlled dissolution of a steel sample, followed by spectrometric measurement of the elements being investigated. At the Filab laboratory, feasibility is assessed according to the requested ASTM E3515 reference, grade, sample form and expected concentrations before testing begins.

Which elements can be investigated in steel using ICP-AES?

The elements being investigated are defined according to your steel grade and inspection objective. ICP-AES is particularly suitable for multi-element determination after dissolution. The elements, concentration ranges and limits of quantification are confirmed by the Filab laboratory during the feasibility study.

Which steel samples can be sent to the Filab laboratory?

Steel parts, coupons, chips, powders and fragments can be sent to the Filab laboratory. The quantity required depends on the sample form, the elements being investigated and the preparation required. Providing the origin and sampling area helps ensure the relevance of the analysis.

Why choose ICP-AES for steel analysis?

ICP-AES is selected for its ability to perform multi-element determination after sample dissolution. Its suitability for your needs is confirmed by the Filab laboratory based on the elements being tested, the expected concentrations, and the requirements of your specification.

How can I request an ASTM E3515 analysis of steel from the Filab laboratory?

To request an analysis, provide the Filab laboratory with the ASTM E3515 reference, the elements to be tested, the nature and number of samples, and your compliance criteria. The Filab laboratory can assess feasibility and direct you to the appropriate service.
The filab advantages
A highly qualified team
A highly qualified team
Responsiveness in responding to and processing requests
Responsiveness in responding to and processing requests
A COFRAC ISO 17025 accredited laboratory
A COFRAC ISO 17025 accredited laboratory
(Staves available on www.cofrac.com - Accreditation number: 1-1793)
A complete analytical facility of 5,200m²
A complete analytical facility of 5,200m²
Tailor-made support
Tailor-made support
Video debriefing available with the expert
Video debriefing available with the expert
Arnaud Joudrain Metallurgical Specialist
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